WO2003053145A1 - Bactericidal composition - Google Patents

Bactericidal composition Download PDF

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Publication number
WO2003053145A1
WO2003053145A1 PCT/JP2002/013293 JP0213293W WO03053145A1 WO 2003053145 A1 WO2003053145 A1 WO 2003053145A1 JP 0213293 W JP0213293 W JP 0213293W WO 03053145 A1 WO03053145 A1 WO 03053145A1
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Prior art keywords
parts
sulfamoyl compound
copies
sulfamoyl
anionic surfactant
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PCT/JP2002/013293
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French (fr)
Japanese (ja)
Inventor
Hiroyuki Suzuki
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Nissan Chemical Industries, Ltd.
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Application filed by Nissan Chemical Industries, Ltd. filed Critical Nissan Chemical Industries, Ltd.
Priority to AU2002354251A priority Critical patent/AU2002354251A1/en
Publication of WO2003053145A1 publication Critical patent/WO2003053145A1/en

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    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/64—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with three nitrogen atoms as the only ring hetero atoms
    • A01N43/647—Triazoles; Hydrogenated triazoles
    • A01N43/653—1,2,4-Triazoles; Hydrogenated 1,2,4-triazoles

Definitions

  • the present invention relates to a fungicide composition
  • a fungicide composition comprising a mixture of a sulfamoyl compound and an active ingredient compound of a known fungicide.
  • WO 99/21851 describes that sulfamoyl compounds have bactericidal activity. Disclosure of the invention
  • the present invention provides the following formula (1):
  • Bok represented by 2 (N, N-dimethylsulfamoyl) -3- [2-methyl-3-bromo - 6 Full Oroindoru - Bok I le] sulfonyl - 1, 2, 4- Toriazoru (hereinafter Surufamoi And a folpet, simoxanil, fosetyl or manzeb as active ingredients.
  • Sulfamoyl compounds are described in WO99211851 and have excellent bactericidal activity.
  • Simoxanil (common name) has the formula (2a): (2a)
  • It is a mixture of a manganese salt of ethylenebisdithiocarbamate and a zinc salt, and is a known fungicide.
  • the hold (generic name) is of the form (2d):
  • N- (trichloromethylthio) phthalimide represented by, and is a known fungicide.
  • the features of the bactericide composition of the present invention are, firstly, that the bactericidal efficacy is clearly enhanced and an immediate bactericidal effect is imparted as compared with the case where each agent is applied alone. Second, it induces a broader germicidal spectrum not found in existing germicides, and a long residual effect. Third, the drug dose can be reduced compared to using each drug alone.
  • the fungicide composition of the present invention has a synergistic fungicidal action.
  • This synergistic bactericidal action is based on a synergistic effect that cannot be predicted from the bactericidal properties of each single agent, and the usefulness of the bactericide composition of the present invention is greater than the use of each drug alone for various diseases. It can be said that there is a certain control effect.
  • the preferred mixing ratio of the sulfamoyl compound and the simoxanil in the fungicidal composition is as follows. L 00 parts by weight, for example, 0.1 to 10 parts by weight.
  • the preferred treatment amount of the fungicidal composition of the sulfamoyl compound and simoxanil depends on the type of the disease to be controlled and the like.
  • the sulfamoyl compound is 0.1 to! O OOga i / ha (however, & 1 11 & represents the number of grams of active ingredient per hectare, the same applies to the following), and the processing amount of cimoxanil from 0.1 to 1 000 ga iZha, for example
  • the former is 1-300 gai / ha, and the latter is l-300ga iZha.
  • a preferable mixing ratio of the sulfamoyl compound and fosetyl in the fungicide composition is that 0.001 to 2000 parts by weight, for example, 0.01 to 500 parts by weight of fosetyl relative to 1 part by weight of the sulfamoyl compound. Parts, for example 0.1 to 100 weight Department.
  • the preferred amount of the disinfectant composition of the sulfamoyl compound and fosetyl depends on the type of the disease to be controlled.
  • the effective amount of the sulfamoyl compound is 0.1 to 1000 gai / ha. 0.1-:! O O O O O g a i / ha Processing amount, for example, the former is l S O O g a iZh a, and the latter is 1-2
  • the preferred mixing ratio of the sulfamoyl compound and manzeb in the fungicide composition is such that the amount of manzeb is, for example, from 0.001 to 1 part by weight of the sulfamoyl compound.
  • 2000 parts by weight for example, 0.01 to 500 parts by weight, for example, 0.1 to 100 parts by weight.
  • the preferred treatment amount of the fungicidal composition of the sulfamoyl compound and manzeb depends on the type of the target disease to be controlled and the like.
  • 0.1 to 1000 gai / ha of the sulfamoyl compound and manzeb are used as the active ingredient.
  • the preferred mixing ratio of the sulfamoyl compound and the holpet in the fungicide composition is such that, for 1 part by weight of the sulfamoyl compound, the holpet is, for example, 0.001 to 2000 parts by weight, for example, 0.01 to 500 parts by weight, For example, 0.1 to 100 parts by weight.
  • the preferred treatment amount of the fungicide composition of the sulfamoyl compound and the holbet depends on the kind of the target disease to be controlled and the like.
  • the sulfamoyl compound is 0.1 to L 000 gaia.
  • the amount of processing for the holpet is 0.1 to: LOOOO gai / ha, for example, the processing amount for the former is l to 300 gaiZha, and the latter is the processing amount for 1 to 2000 gaiZha.
  • the fungicidal composition of the present invention can be applied to so-called agricultural diseases that damage agricultural and horticultural crops and trees. Diseases that can be controlled using the fungicide composition of the present invention include, but are not limited to, the following.
  • Diseases include rice blast (Py riculariaoryzae), and rice leaf blight (Coc hli obo lus mi yab e anus). Disease (Rh izoct on iaso 1 ani) Powdery mildew of wheat (Ery siphegr am inisf.sp.ho rdei, f.sp, tritici), Leaf spot (Py re nopho ragr am inea) (Py re noph
  • Nipirim mepanipyrim
  • mepronilile mepronil metalaxyl (metalaxyl), metconazole (metconazole), methasulfocarb (methasulfocarb), metiram (metirain), metominostrobin (metominostrobin), microbuinil (myclobutan53), TF (Test name), mebenil, mecarb inzid, mercuric chloride, mercuric oxide Oner curic ox ide, mercurous chloride, metalaxylol M) , Metam, metalazoxolon, methasul focarb, methfuroxam, methyl bromide, methyl isothiocyanate, methyl mercury benzoate (methylmercury benzoate), methylmercury dicyandiamide, metrafenone, methos refobax
  • pyraclostrobin pyridinitril (pyridini tri 1), pyroxycycloa (pyroxychlor), pyroxysulfur (pyroxyfur), phenylphenol (2-phenylphenol), quinometi Quinomethionate, quinoxyfen, quintozene, quinacetol, quinazamide, quinazamid, quinconazole, rabenzazole, sodium hydrogen carbonate, next Sodium hypochlorite, sulfur (sul fur), spiroxamine (spiroxamine), salicylanilide (sal icylani 1 ide), silthiofam (silthiofam), simeconazole, sodium azide (sodium azide), sodium azide J Lettophenylelephenoxide (sodium orthophenylphenoxide), sodium pentachlorophenoxide (sodium pentachlorophenoxide), sodium polysulfide (sodium polysulfide), streptomycin (streptomycin
  • the mixture of the sulfamoyl compound described in the present application and the bactericide also has a good bactericidal activity. Shows sex.
  • the synergistic germicidal effect of the germicidal composition can be explained as follows. That is, the individual active compounds often exhibit their bactericidal activity in each case, but in this case the bactericidal activity of the combination of the two active compounds is simply the sum of the activities of each of the two compounds ( This is referred to as synergism when it is greater than the expected activity).
  • the expected activity of a particular combination of two fungicides can be calculated as follows. (Colby SR> Calculation of synergistic and antagonistic reaction of herbicide combinations, see Weed, Vol. 15, pages 20-22 (1967))
  • the bactericide composition of the present invention When using the bactericide composition of the present invention, it is usually mixed with a suitable solid carrier or liquid carrier, and if necessary, a surfactant, a penetrant, a spreading agent, a thickener, a deicing agent, a binder, Add anti-caking agent, disintegrant, defoamer, preservative, decomposition inhibitor, etc.
  • ⁇ soluble concentrate emulsion (emulsifiable concentrate), 7 wettable powder, ⁇ solvent (water soluble powder), water dispersible granule, water soluble granule, suspension Preparation (concentrated emulsion), suspoemulsion (suspoemulsion), microemulsion, dustable powder, granule and gel, etc. It can be put to practical use as a formulation.
  • the preparation of any of the above dosage forms can be provided in a water-soluble package such as a water-soluble capsule or a bag of a water-soluble film.
  • solid carriers examples include quartz, kaolinite, pyrophyllite, sericite, talc, bentonite, acid clay, attapulgite, zeolite, and diatomaceous earth.
  • Natural minerals, inorganic salts such as calcium carbonate, ammonium sulfate, sodium sulfate and chloride chloride, synthetic silica and synthetic silicate.
  • liquid carrier examples include alcohols such as ethylene glycol, propylene glycol and isopropanol; aromatic hydrocarbons such as xylene, alkylbenzene and alkylnaphthalene; ethers such as butyl sorbate; and ketones such as cyclohexanone.
  • esters such as N-methylpyrrolidone, acid amides such as N-methylpyrrolidone and N-octylpyrrolidone, vegetable oils such as soybean oil, naney oil, cottonseed oil and castor oil, and water.
  • solid and liquid carriers may be used alone or in combination of two or more.
  • the surfactant include polyoxyethylene alkyl ether, polyoxyethylene alkylaryl ether, polyoxyethylene styrene phenyl ether, polyoxyethylene polyoxypropylene block copolymer, polyoxyethylene fatty acid ester, sorbitan fatty acid ester And nonionic surfactants such as polyoxyethylene sorbin fatty acid esters, alkyl sulfates, alkyl benzene sulfonates, lignin sulfonates, alkyl sulfosuccinates, naphthalenes; V levonates, alkyl naphthalene sulfonic acids Salt, salt of formalin condensate of naphthylene sulfonic acid, salt of formalin condensate of alkyl naphthalene sulfonic acid, polyoxyethylene alkyl aryl ether sulfate and phosphate
  • the content of these surfactants is not particularly limited, but is usually preferably in the range of 0.05 to 20 parts by weight based on 100 parts by weight of the preparation of the present invention. These surfactants may be used alone or in combination of two or more.
  • composition examples of the present invention are not limited to these.
  • parts Means part by weight.
  • Fungicide composition of the present invention 0 1 to 80 parts
  • an anti-caking agent and an anti-decomposition agent [emulsifiable concentrate]).
  • Fungicide composition of the present invention 0.1 to 30 parts
  • Fungicide composition of the present invention 0.1 to 70 parts
  • Fungicide composition of the present invention 0.1 to 90 parts
  • the fungicide composition of the present invention 0.01 to 70 parts
  • the fungicide composition of the present invention 0.01 to 80 parts
  • Other examples include a binder and a decomposition inhibitor.
  • the fungicide composition of the present invention 0.01 to 30 parts
  • anti-drift agent examples include an anti-drift agent and an anti-decomposition agent.
  • the above-mentioned preparations are diluted with water 1 to 10,000 times or not, so that the active ingredient becomes 0.0001 to 50 kg, preferably 0.001 to 10 kg per hectare (ha). Spray.
  • agrochemical preparations containing the fungicide composition of the present invention as an active ingredient will be specifically described, but the present invention is not limited thereto.
  • “parts” means parts by weight.
  • HLB represents a value obtained by the Griffin equation.
  • the above is uniformly mixed and pulverized to obtain a wettable powder.
  • Nonionic surfactant Kao Corporation
  • the above is uniformly mixed and pulverized to obtain a powder.
  • the above is uniformly mixed and pulverized to obtain a wettable powder.
  • Nonionic surfactant Kao Corporation
  • the above is uniformly mixed and pulverized to obtain a powder.
  • the above is uniformly mixed and pulverized to obtain a wettable powder.
  • Nonionic surfactant Kao Corporation
  • a wet powder frame is used as a suspension.
  • the above is uniformly mixed and pulverized to obtain a powder.
  • Nonionic surfactant Kao Corporation
  • the above is uniformly mixed and pulverized to obtain a powder.
  • composition of the present invention is not limited only to these.
  • Test example 1 Grape downy mildew control effect test
  • Control value [11 (area ratio of treated spot / area ratio of untreated section)] XI 00
  • Table 1 Table 1
  • Test Example 4 Potato disease control effect test
  • a potato (cultivar: Danshak) grown in a pot with a diameter of 7 cm was diluted with water to prepare a solution of the fungicidal composition of the present invention prepared according to Formulation Example 8 so that each drug solution was prepared to have a respective dose.
  • 10 ml was sprayed per pot.
  • a spore suspension (2 ⁇ 10 5 ml) of potato blight fungus (Phytophthora infestans) was sprayed and placed in an inoculation box at a temperature of 20 ° C and a humidity of 95% or more.
  • the ratio of the area of the lesion formed after 5 days to the inoculated leaves was measured, and the control value was calculated according to the formula in Test Example 1 and the same formula.
  • Test Example 6 Test for controlling potato blight
  • Test Example 7 Test for controlling potato blight
  • Potatoes (variety: Danshak) grown in pots with a diameter of 15 cm are sprayed with a spore suspension of potato blight (Phytophthora infestans) (211, 1111). I put in for 6 hours. After air-drying, the formulation of the bactericide composition of the present invention prepared according to Formulation Example 16 was diluted with water, and a chemical solution adjusted to each concentration was sprayed at 10 ml per pot using a spray gun. Thereafter, the cells were placed again under humidification conditions, the ratio of the lesion area formed 5 days after the inoculation to the inoculated leaves was measured, and the control value was calculated according to the same formula as that of Test Example 1.
  • Table 7 shows the results.
  • E represents the expected value in Colby's equation. (Table 1) Drug Drug dosage ⁇ gai / ha) Control value E
  • Simoxanil 150 75 The composition of the present invention exhibits an excellent synergistic bactericidal effect and shows no phytotoxicity to useful crops, and is therefore useful as an agricultural and horticultural fungicide.

Abstract

A novel bactericidal composition characterized by containing as active ingredients 1-(N,N-dimethylsulfamoyl)-3-[2-methyl-3-bromo-6-fluoroindol-1-yl]sulfonyl-1,2,4-triazole, which is represented by the formula (1), (1) and any of folpet, cymoxanil, fosetyl, and manzeb.

Description

明細書  Specification
殺菌剤組成物 技術分野  Fungicide composition Technical field
本発明は、 スルファモイル化合物と、 公知の殺菌剤の有効成分化合物とを混合し てなることを特徴とする殺菌剤組成物に関するものである。 背景技術  The present invention relates to a fungicide composition comprising a mixture of a sulfamoyl compound and an active ingredient compound of a known fungicide. Background art
WO 9 9 / 2 1 8 5 1には、 スルファモイル化合物が殺菌活性を有することが記 載されている。 発明の開示  WO 99/21851 describes that sulfamoyl compounds have bactericidal activity. Disclosure of the invention
本発明者らは、 優れた殺菌剤を開発すべく種々検討を重ねた結果、 本発明を完成 させた。 すなわち、 本発明は、 式 （1 )：  The present inventors have conducted various studies to develop an excellent bactericide, and as a result, completed the present invention. That is, the present invention provides the following formula (1):
Figure imgf000003_0001
2 で表される卜 （N, N-ジメチルスルファモイル） -3- 〔2-メチル -3-ブロム- 6-フル ォロインドール-卜ィル〕 スルホニル- 1, 2, 4-トリァゾール （以下、 スルファモイ ル化合物と称する。） とホルペット、 シモキサニル、ホセチルまたはマンゼブとを有 効成分として含有することを特徴とする殺菌剤組成物である。
Figure imgf000003_0001
Bok represented by 2 (N, N-dimethylsulfamoyl) -3- [2-methyl-3-bromo - 6 Full Oroindoru - Bok I le] sulfonyl - 1, 2, 4- Toriazoru (hereinafter Surufamoi And a folpet, simoxanil, fosetyl or manzeb as active ingredients.
スルファモイル化合物は、 W〇 9 9 2 1 8 5 1に記載されており、 優れた殺菌 活性を有している。  Sulfamoyl compounds are described in WO99211851 and have excellent bactericidal activity.
シモキサニル （一般名） は式 （2 a ) ： (2a)Simoxanil (common name) has the formula (2a): (2a)
Figure imgf000004_0001
で表されるトランス— 1一 （2 _シァノ _ 2—メトキシイミノアセチル） 一3—ェ チルゥレアであり、 公知の殺菌剤である。
Figure imgf000004_0001
Trans-11- (2-cyano-2-methoxyiminoacetyl) -13-ethylperia, which is a known fungicide.
ホセチル （一般名） は式 （2 b) ：  Josetil (generic name) is of formula (2b):
Figure imgf000004_0002
で表されるアルミニウムトリス （ェチルホスホナ一ト） であり、 公知の殺菌剤であ る。
Figure imgf000004_0002
It is aluminum tris (ethyl phosphonate) represented by and is a well-known fungicide.
マンゼブ （一般名） は式 （2 c) ：  Manzeb (common name) is expressed by the formula (2c):
nxZnv (2c)
Figure imgf000004_0003
nxZnv (2c)
Figure imgf000004_0003
で表されるエチレンビスジチォカーバモェ一トマンガン塩と亜鉛塩との混合物であ り、 公知の殺菌剤である。 It is a mixture of a manganese salt of ethylenebisdithiocarbamate and a zinc salt, and is a known fungicide.
ホルぺット （一般名） は式 （2 d) :
Figure imgf000005_0001
The hold (generic name) is of the form (2d):
Figure imgf000005_0001
で表される N— (トリクロロメチルチオ） フタルイミドであり、 公知の殺菌剤であ る。 N- (trichloromethylthio) phthalimide represented by, and is a known fungicide.
本発明殺菌剤組成物の特徴は、 第 1に各薬剤の単独での施用の場合に比べ、 その 殺菌効力が明らかに増強されるとともに即効的な殺菌効果が付与されることである。 第 2に、 既存の殺菌剤に観られない広い殺菌スペクトラムや、 長い残効性が誘導さ れることである。 第 3に、 各薬剤を単独で使用した場合に比べ、 投下薬量を低下さ せうることである。  The features of the bactericide composition of the present invention are, firstly, that the bactericidal efficacy is clearly enhanced and an immediate bactericidal effect is imparted as compared with the case where each agent is applied alone. Second, it induces a broader germicidal spectrum not found in existing germicides, and a long residual effect. Third, the drug dose can be reduced compared to using each drug alone.
即ち、 本発明殺菌剤組成物は、 相乗的殺菌作用を有するものである。 この相乗的 殺菌作用は各単剤の有する殺菌特性からは予測し得ぬ相乗効果に基づくもので、 本 発明殺菌剤組成物の有用性は各種病害に対して各薬剤を単独で使用するよりも確実 な防除効果を発揮し得る点にあるといえる。  That is, the fungicide composition of the present invention has a synergistic fungicidal action. This synergistic bactericidal action is based on a synergistic effect that cannot be predicted from the bactericidal properties of each single agent, and the usefulness of the bactericide composition of the present invention is greater than the use of each drug alone for various diseases. It can be said that there is a certain control effect.
スルファモイル化合物とシモキサニルとの殺菌剤組成物における両者の好適な混 合割合は、 スルファモイル化合物の 1重量部に対して対してシモキサニルが例えば 0. 001〜： L 000重量部、 例えば 0. 01〜： L 00重量部、 例えば 0. 1〜1 0重量部である。  The preferred mixing ratio of the sulfamoyl compound and the simoxanil in the fungicidal composition is as follows. L 00 parts by weight, for example, 0.1 to 10 parts by weight.
スルファモイル化合物とシモキサニルとの殺菌剤組成物の好ましい処理薬量は防 除すべき対象病害の種類などにより左右されるが、 例えば有効成分としてスルファ モイル化合物が 0. 1〜：！ O OOga i/ha (但し、 & 1 11&は1へクタ一 ルあたりの活性成分のグラム数を表す、 以下も同様。）、 シモキサニルが 0. 1〜1 000 g a iZh aとなる処理量、 例えば前者が 1〜300 g a i /h aであり、 後者が l〜300ga iZhaとなる処理量等が挙げられる。  The preferred treatment amount of the fungicidal composition of the sulfamoyl compound and simoxanil depends on the type of the disease to be controlled and the like. For example, as the active ingredient, the sulfamoyl compound is 0.1 to! O OOga i / ha (however, & 1 11 & represents the number of grams of active ingredient per hectare, the same applies to the following), and the processing amount of cimoxanil from 0.1 to 1 000 ga iZha, for example The former is 1-300 gai / ha, and the latter is l-300ga iZha.
スルファモイル化合物とホセチルとの殺菌剤組成物における両者の好適な混合割 合は、 スルファモイル化合物の 1重量部に対して対してホセチルが例えば 0. 00 1〜2000重量部、 例えば 0. 01〜500重量部、 例えば 0. 1〜100重量 部である。 A preferable mixing ratio of the sulfamoyl compound and fosetyl in the fungicide composition is that 0.001 to 2000 parts by weight, for example, 0.01 to 500 parts by weight of fosetyl relative to 1 part by weight of the sulfamoyl compound. Parts, for example 0.1 to 100 weight Department.
スルファモイル化合物とホセチルとの殺菌剤組成物の好ましい処理薬量は防除す べき対象病害の種類などにより左右されるが、 例えば有効成分としてスルファモイ ル化合物が 0. ：!〜 1000 g a i/h a、 ホセチルが 0. 1〜：！ O O O O g a i /haとなる処理量、 例えば前者が l S O O g a iZh aであり、 後者が 1〜 2 The preferred amount of the disinfectant composition of the sulfamoyl compound and fosetyl depends on the type of the disease to be controlled. For example, the effective amount of the sulfamoyl compound is 0.1 to 1000 gai / ha. 0.1-:! O O O O g a i / ha Processing amount, for example, the former is l S O O g a iZh a, and the latter is 1-2
000 g a i/h aとなる処理量等が挙げられる。 000 g a i / ha, and the like.
スルファモイル化合物とマンゼブとの殺菌剤組成物における両者の好適な混合割 合は、 スルファモイル化合物の 1重量部に対して、 マンゼブが例えば 0. 001〜 The preferred mixing ratio of the sulfamoyl compound and manzeb in the fungicide composition is such that the amount of manzeb is, for example, from 0.001 to 1 part by weight of the sulfamoyl compound.
2000重量部、 例えば 0. 01〜500重量部、 例えば 0. 1〜100重量部で ある。 2000 parts by weight, for example, 0.01 to 500 parts by weight, for example, 0.1 to 100 parts by weight.
スルファモイル化合物とマンゼブとの殺菌剤組成物の好ましい処理薬量は防除す べき対象病害の種類などにより左右されるが、 例えば有効成分としてスルファモイ ル化合物が 0. 1〜： 1000 g a i/h a、 マンゼブが 0. 1〜： 10000 g a i Zh aとなる処理量、 例えば前者が 1~300 g a i /h aであり、 後者が 1〜 5 000 g a i/h aとなる処理量等が挙げられる。  The preferred treatment amount of the fungicidal composition of the sulfamoyl compound and manzeb depends on the type of the target disease to be controlled and the like. For example, as the active ingredient, 0.1 to 1000 gai / ha of the sulfamoyl compound and manzeb are used. 0.1 to: A processing amount of 10000 gai / Zha, for example, a processing amount of 1 to 300 gai / ha for the former and 1 to 5,000 gai / ha for the latter.
スルファモイル化合物とホルペットとの殺菌剤組成物における両者の好適な混合 割合は、 スルファモイル化合物の 1重量部に対して、 ホルペットが例えば 0. 00 1〜2000重量部、 例えば 0. 01〜500重量部、 例えば 0. 1〜 100重量 部である。  The preferred mixing ratio of the sulfamoyl compound and the holpet in the fungicide composition is such that, for 1 part by weight of the sulfamoyl compound, the holpet is, for example, 0.001 to 2000 parts by weight, for example, 0.01 to 500 parts by weight, For example, 0.1 to 100 parts by weight.
スルファモイル化合物とホルべッ卜との殺菌剤組成物の好ましい処理薬量は防除 すべき対象病害の種類などにより左右されるが、 例えば有効成分としてスルファモ ィル化合物が 0. 1〜： L 000 g a i a、 ホルペットが 0. 1〜： L O O O O g a i/h aとなる処理量、 例えば前者が l〜300 g a iZh aであり、 後者が 1 〜2000 g a iZh aとなる処理量等が挙げられる。  The preferred treatment amount of the fungicide composition of the sulfamoyl compound and the holbet depends on the kind of the target disease to be controlled and the like. For example, as the active ingredient, the sulfamoyl compound is 0.1 to L 000 gaia. The amount of processing for the holpet is 0.1 to: LOOOO gai / ha, for example, the processing amount for the former is l to 300 gaiZha, and the latter is the processing amount for 1 to 2000 gaiZha.
本発明殺菌剤組成物は農園芸作物および樹木などを加害するいわゆる農業病害に 対して適用できる。 本発明殺菌剤組成物を用いて防除しうる病害には具体的には次 に示すものがあるが、 それらのみに限定されるものではない。  The fungicidal composition of the present invention can be applied to so-called agricultural diseases that damage agricultural and horticultural crops and trees. Diseases that can be controlled using the fungicide composition of the present invention include, but are not limited to, the following.
すなわち、 病害としては、 イネのいもち病 （Py r i c u l a r i a o r y z a e )、 ご 葉枯炳 (Coc h l i obo l u s mi yab e anu s) 紋枯 病 (Rh i z o c t on i a s o 1 a n i ) ムギ類のうどんこ病 (E ry s i p h e g r am i n i s f . s p. ho r d e i , f . s p， t r i t i c i ), 斑葉病 (Py r e nopho r a g r am i n e a),網斑病 (Py r e nophDiseases include rice blast (Py riculariaoryzae), and rice leaf blight (Coc hli obo lus mi yab e anus). Disease (Rh izoct on iaso 1 ani) Powdery mildew of wheat (Ery siphegr am inisf.sp.ho rdei, f.sp, tritici), Leaf spot (Py re nopho ragr am inea) (Py re noph
0 r a t e r e s), 赤かび病 (G i b b e r e 1 1 a z e a e)、 さび病 ( P u c c i n i a s t r i i f o rmi s, P. g r am i n i s , P. r e c o n d i t a , P. ho r d e i ), 雪腐病 (T i p u 1 a s p.， M i c r on e c t r i e 1 l a n i v a i s ), 裸黒穂病 (U s t i 1 a g o t r i t i c0 rateres), Fusarium head blight (G ibbere 1 1 azeae), Rust (P ucciniastriifo rmi s, P. gr am inis, P. recondita, P. ho rdei), Snow rot (T ipu 1 as p., M icr on ectrie 1 lanivais), smut (U sti 1 agotritic)
1， U. n u d a)、 アイスポット (P s eu.do c e r c o s po r e 1 l a h e r p o t r i c ho i d e s)、 雲形病 (Rhyn c ho s p o r i um s e c a 1 i s )、 葉枯病 (S e p t o r i a t r i t i c i)、 ふ枯病 (L e p t o s p h a e r i a nod o r um)、力ンキッの黒点病 (D i apo r t he c i t r i)、 そうか病 （E 1 s i no e f awe e t t i)、 果実腐敗病 （P e n i c i 1 1 i um d i g i t a l um, P. i t a l i c um)、 リンゴのモニ リァ病 (S e l e r o t i n i a ma l i)、 腐らん病 (V a 1 s a ma 1 i )、 うどんこ病 (Podo s ph a e r a l c uc o t r i c h a),斑点落葉病 (A1, U. nuda), eye spot (Ps eu.do cercos po re 1 laherpotric ho ides), scald disease (Rhyn c ho spori um seca 1 is), leaf blight (Septoriatritici), blight (L eptosphaeria nod or um), black spot of rickets (Diaport he citri), scab (E1 si no ef awe etti), fruit rot (Penici 11 1 um digital um, P. italic um) ), Apple Monilia disease (Selerotinia ma li), rot (Va1 sa ma1i), powdery mildew (Podo s ph aeralc uc otricha), spotted leaf spot (A
1 t e r n a r i a ma l i)、 黒星炳 (V e n t u r i a i n a e q u a 1 i s), ナシの黒星病 （Ve n t u r i a n a s h i c o l a)、 黒斑病 （A 1 t e r n a r i a k i ku c h i an a)> 赤星病 (Gymno s p o r ang i um ha r a c anum)、 モモの灰星病 (S c 1 e r o 1 i n i a c i n e r e a )、 黒星病 (C l e ado s po r i um c a r poph i l um)、 フォ モプシス腐敗病 （Phomop s i s s p.), ブドウのベと病 （P 1 a s mo p a r a v i t i c o l a)、 黒とっ炳 (E l s i no e ampe l i na)、 晚 腐病 (G 1 ome r e 1 1 a c i ngu l a t a)、 うどんこ病 (U n c i n u l a n e c a t o r ), さび病 (Ph ak op s o r a amp e l o s i d i s )、 力キの炭そ病 （G l oe o s po r i um k a k j )、 落葉病 （Ce r e o s po r a k a k j , My c o s ph a e r e l 1 a n awa e)、 ゥリ類 のべと病 (P s e udop e r e no s po r a c ub e n s i s)、 炭そ病 (C o l l e t o t r i c hum l a g e n a r i um)、 うどんこ病 (S p h a e r o t he c a f u 1 i g i n e a)> つる枯病 (My c o s ph a e r e 1 1 a me l on i s)、 卜マ卜の疫病 (Phy t oph t ho r a i n f e s t a n s )、 輪紋病 （A l t e r n a r i a s o l an i)、 葉かび病 (C 1 a d o s po r i um f u l vum)、 ナスの褐紋病 (Phomo p s i s v e x a n s )、 うどんこ病 （E r y s i ph e c i c ho r a c o a r um), アブラナ 科野菜の黒斑病 （A l t e r n a r i a j ap on i c a)、 白斑病 （Ce r e o s p o r e 1 l a b r a s s i c a e),不千のさび病 (P u c c i n i a a 1 1 i i )、 ダイズの紫斑病 （Ce r c o s po r a k i ku c h i i)、 黒とう 病 (E l s i no e g l yc i ne s)、 黒点病 (D i a p o r t h e p h a s e o 1 o 1 um), ィンゲンの炭そ病 (Co l l e t o t r i c hum l i n d emu t h i anum)、 ラッカセィの黒渋 ί)丙 (My c o s p ha e r e l l a p e r s on a t um)> 褐斑炳 (Ce r c o s po r a a r a c h i d i c o 1 a)、 エンドゥのうどんこ病 （E r y s i ph e p i s i)、 ジャガイモの夏疫 病 （A l t e r n a r i a s o l an i)、 ィチゴのうどんこ病 (S p h a e r o t h e c a humu l i)、 チヤの網もち病 (Exo b a s i d i um r e t i c u 1 a t um)、 白星病 （E l s i no e l eu c o s p i l a), タノ コ の赤星病 （A l t e r n a r i a l i ng i p e s)、 うどんこ病 (E r y s i p h e c i c ho r a c e a r um), 灰そ病 (Co l l e t o t r i c hum t a b a c um)、 テンサイの褐斑病 (Ce r c o s po r a b e t i c o 1 a), ノ ラの黒星病 (D i p l o c a r p on r o s a e), うどんこ病 (S p h a e r o t he c a p a n n o s a)> キクの te斑病 （S e p t o r i a c h r y s an t hemi i nd i e i)、 白さび病 (P u c c i n i a ho r i an a)、 種々の作物の灰色かび病 (B o t r y t i s c i n e r e a) および種々の作物 の菌核病 （S c l e r o t i n i a s c l e r o t i o r um) 等が挙げられる。 また、 本発明殺菌剤組成物は、 更にもう 1種以上の公知の殺菌剤と混合すること もできる。 そのような殺菌剤について、 具体的にその一般名を例示すれば次の通り であるが、 必ずしもこれらのみに限定されるものではない。 1 ternaria ma li), Bung Kuroboshi (Venturiainaequa 1 is), Pear scab (Ve nturianashicola), Black spot (A 1 ternariaki ku chi an a)> Red scab (Gymno spor ang i um ha rac anum), Peach ash disease (S c 1 ero 1 iniacinerea), black scab (Cle ado s po ri um car poph il um), Phomopsis rot (Phomop siss p.), Grape downy mildew (P 1 as mo paraviticola), black tobitsu (E lsi no e ampe li na), 晚 rot (G 1 ome re 1 1 aci ngu lata), powdery mildew (Uncinulanecator), rust (Ph ak op sora amp elosidis) , Anthracnose of iki (Gloe os po ri um um kakj), Deciduous disease (Ce reos po rakakj, My cos ph aerel 1 an awa e), Downy mildew of perilla (P se udop ere no s) po rac ub ensis), Anthracnose (Colletotric hum lagenari um), Powdery mildew (S phaerot he cafu 1 iginea)> Vine blight (My cos ph aere 1 1) a me l on is), Phytoph t ho rainfestans, Ring stalk (A lternariasol an i), Leaf mold (C 1 ados po ri um ful vum), Brown spot of eggplant (Phomo psisvexans), powdery mildew (Erysi ph ecic ho racoar um), black spot on cruciferous vegetables (A lternariaj ap on ica), white spot (Ce reospore 1 labrassicae), scab rust (P ucciniaa) 1 1 ii), soybean purpura (Cercos po raki ku chii), black spot (E lsi no egl yc i ne s), black spot (Diaporthephaseo 1 o 1 um), lletotric hum lind emu thi anum), black astringency of laccasei i) hei (My cosp ha erellapers on at um)> brown spot (Cercos po raarachidico 1a), endo powdery mildew (E rysi ph episi), potato Summer blight (A lternariasol an i), strawberry powdery mildew (S phaerotheca humu li), cilia net blight (Exo basidi um reticu 1 at um), white scab (E lsi no el eu cospila), Tano Red scab (A lternariali ng) ipes), powdery mildew (E rysiphecic ho racear um), scab (Colletotric hum tabac um), brown spot of sugar beet (Cercos po rabetico 1a), black scab (D iplocarp on rosae) , Powdery mildew (S phaerot he capannosa)> chrysanthemum te spot (Septoriachrys an t hemi i nd iei), white rust (P uccinia ho ri an a), gray mold on various crops (Botrytiscinerea) And sclerotium disease of various crops (S clerotiniasclerotior um). Further, the fungicide composition of the present invention can be further mixed with at least one other known fungicide. Specific examples of such general names for such disinfectants are as follows, but are not necessarily limited thereto.
ァシベンゾラルー S—メチル（adbenzolar- S-methyl)、 ァシルァミノべンザミド (acylaminobenzamide)、 ァシぺタックス cypetacs), ァ レジモリレフ (aldimorph), アンバム（amobam)、 アムプロピルホス （a即 ropyfos)、 了二ラジン (anilazine)、 ァ リルアルコール （allyl alcohol), ァウレ口ファンジン （aureofungin)、 ァザコナ ソーリレ（azaconazole)、アジチラム、 azi thiram)、ァゾキシスト口ビン (azoxystrobin)、 バリウムポリサルファイド (barium polysulfide), ベナラキシル (benalaxyl), ベ ノダニル （benodanil)、 べノミル （benomyl)、 ベンキノックス （benquinox)、 ベン 夕ルロン (bentaluron), ベンチアバリカルプ (benthiaval icarb), ベンチアゾール (benthiazole), ベンザルコニゥムクロライド （benzalkonium chloride)、 ベンザマ クリル （benzamacril)、 ベンズァモルフ （benzamorf)、 ベンゾハイドロキサミック ァシド (benzohydroxamic acid),ビナノ クリリレ (binapacryl)、ヒフェ二レ (biphenyl)、 ビテル夕ノール （bitertanol)、 ビチォノール （bithionol)、 ベトキサジンS-methyl (adbenzolar- S-methyl), acylaminobenzamide (acylaminobenzamide), cypetacs (ascidax), aldimorph (aldimorph), amobam (ambam), ampropylphos (aro ropyfos), ryujirazine ( anilazine) Allyl alcohol, aureofungin, azakona sorile (azaconazole), azitiram, azi thiram, azoxystrobin, azoxystrobin, barium polysulfide, benalaxyl, benodanil ), Benomyl, benquinox, bentaruron, benthiaval icarb, benthiazole, benzalkonium chloride, benzamacril ), Benzamorph (benzamorf), benzohydroxamic acid, benzohydroxamic acid, binapacryl, biphenyl, biteranol, bithionol, bitoxazine
(bethoxazine) , ホノレド——液 (bordeaux mixture) > ブラス 卜サイジン一 S(bethoxazine), honoledo --- liquid (bordeaux mixture)
(blast icidin_S)、ブロモコナゾ——Jレ (bromoconazole)、フヒリメ——卜 (bupirimate ブチオベート （buthiobate)、 ブチルァミン （butylamine)、 カルシウムポリスルフ ィ ド (calcium olysulfide)^ キヤプ夕フォール (captafol), キャフタン (captan), カッパ一ォキシクロリド （copper oxychloride)、 カルプ口パミド （cai"propamid)、 力ルバモルフ （carbamoi"ph)、 カルベンダジン （carbendazim)、 カルポキシン(blast icidin_S), bromoconazole—J (bromoconazole), bupirimate (buthiobate), butyramine (butylamine), calcium polysulfide (calcium olysulfide) ^ captafol, captan ), Copper oxychloride, carp mouthpamide (cai "propamid), carbamoi" ph, carbendazim, carpoxin
(carboxin)、 カルホン (carvone), チェシユントミクスチヤ (Cheshunt mixture)、 キノメチォネート （chinomethionat)、 クロベンチァゾン （chlobenthiazone)、 クロ ラニフォルメタン （Chloranifonnethane)、 クロラニル （Chloranil)、 クロルフエナ ゾール (chlorfenazol), クロロネブ (chloroneb), クロロピクリン (Chloropicrin), クロ口夕ロニル （chlorothalonil) クロロキノックス （Chlorquinox)、 クロゾリネ ート （chlozolinate)、 クリムバゾール （Climbazole)、 クロ トリマゾール(carboxin), carvone, Cheshunt mixture, chinomethionate, chlobenthiazone, Chloranifonnethane, Chloranil, Chlorfenazol chloroneb), chloropicrin, chlorothalonil Chlorquinox, chlozolinate, climbazole, clotrimazole
(Clotrimazole),カツノヽ0—ァセテエイト (copper acetate) ,塩 ¾te炭酸銅 ^copper carbonate, basic), τΚ酸ィ匕第二銅 (copper hydroxide),力ッノ ——ナフ夕レン ^copper naphthenate), カツノ ——オレアイト (copper oleate), 硫酸銅 opper sul fate)> 塩基性硫酸銅 （copper sulfate, basic), カッパ一ジンククロメイト （copper zinc chromate)> クレゾール（cresol)、 クフラネフ （cufraneb)、 クプロバム （cuprobam)、 シァゾフアミド (cyazofamid)、 シクラフ Jレアミド (cyclafuramid)、 シクロへキシ ミ F (cycloheximide) シフ Jレフェナミ H (cyf lufenamid),シモキサニル (cymoxanil)、 サイペンダソーノレ cypendazole)、 シプ Γ3コナソーリレ cyproconazol)、 シプ□ジニ リレ （cyprodini 1)、 シプロフラム （cyprofuram)、 ダゾメット（dazomet)、 デ一ビーシ 一ピー （DBCP)、 デバカルプ （debacarb)、 デカフェンチン （Decaf ent in)、 デハイド ロアセティ ト （dehydroacetic acid) , ジクロン （dichlone) ジクロロフェン (dichlorophen) , ジクロゾリ ン （ dichlozol ine )、 ジク ロブトラゾール (diclobutrazol),ジクロフラニド (dichlofluanid)、 ジクロメジン (diclomedine)、 ジクロラン （dicloran)、 ジエトフェンカルプ （diethofencarb)、 ジェチルピロカル ポネィ卜 （diethyl pyrocarbonate)、 ジクロシメッ卜 （diclocymet)、 ジフエノコナ ソーリレ (di fenoconazole)、 ジフ レメ 卜リン (di f lumetor im) , ジメチリモーリレ ( dimethirimol )、 ジメ トモルフ ( d i met homo rph ) , ジモキシス'卜ロビン (dimoxystrobin) > ジニコナゾ一 Jレ （diniconazole)、 ジニコナゾ一 レー M (diniconazole— M)、 ジノブトン (dinobuton) ジノカップ (dinocap), ジノカップ —4 (dinocap-4)、 ジノカップ一 6 (dinocap-6), ジノクトン (dinoctoiu、 ジノス ルフォン （dinosulfon)、 ジノテルボン （dinoterbon)、 ジフエ二ルァミン ι,αί phenyl amine;,ジピリチオン (dipyrithione八 ジノスリレフィラム (disulf iram), ジタリムホス （ditalimfos)、 ジチアノン （dithianon)、 デーェヌォ一シ一 （DN0C)、 ドデ iリレフ (dodemorph), ドジン (dodine 、 ドラゾクソロン (drazoxolon), ェテ フエノホス （edifenphos)、 エポキシコナゾール （epoxiconazole)、 エタコナゾール (etaconazole)、 ェチリモ レ (ethirimol)、 ェ卜リジァノ一ル (etridiazole)、 X テム （Etem)、 エトキシキン （Ethoxyquin)、 ェチルマ一キュリーァセティ ト (ethylmercury acetate) ,ェチレマ——キユリ——ブロマイド、ethylmercury bromide)、 塩化メチル水銀 （ethylmercury chloride), ェチルマ一キュリーフォスフェイ ト (ethylmercury phosphate) ファモキサドン ( famoxadone) > フエナリモル (fenarimol)、 フエブコナソ*ーレ (febuconazole 、 フエナミドン (fenamidone), フェンダゾスラム（fendazosulam)、 フェンフラム （fenfuram)、 フェンへキサミド (fenhexamid), フエノキサニル（fenoxani 1)、 フェンピクロニル （fenpicloni 1)、 フェンプロビジン （fenpropidin)、 フェンプロピモルフ （fenpropimo卬 h)、 フェン チン （fentin)、 フェルバン （ferbam)、 フェリムゾン （ferimzone)、 フルアジナム (fluazinam), フルジォキソニル (f ludioxonil), フルォロイミド (f luoroimide), フルキンコナゾ一ル (fluquinconazole), フルシラゾール (f lusi lazole), フルス ルフアミド （flusulfamide)、 フルトラニル （flutolanil)、 フルトリアフォール (flutriafol) フオルペット （folpet)、 ホセチル—アルミニウム （fosety卜 aluminium), フべリダゾール （fuberidazole)、 フララキシル （furalaxyl)、 フラメ トピル（furametpyr)、フエナミノスルフ（fenaminosul f)、フエナパニル（fenapani 1)、 フエニトロパン （fenitropan)、 フエノキサニル （ fenoxani 1 )、 フルメトバー (flumetover), フルモルフ (flumorph), フルオトリマゾ一ル (f luotrimazole), フルォキサストロビン (fluoxastrobin), フラメ卜ピル (fur匿 tpyr)、 フル力ルバ ニル （furcarbanil)、 フルコナゾール （furconazole)、 フルコナゾ一ルーシス ( furconazole— cis)、 フ レメシク tnックス uurmecycloxリ、 フロファ不——卜 (furophanate), グァザチン (guazatine), グリオジン (glyodin), グリセオフル ビン （griseofulvin)、 へキサクロ口ベンゼン （hexachlorobenzene)、 へキサコナゾ 一 Jレ (hexaconazole)、 ヒメキサソ——Jレ (hymexazol)、ゾ、ラクリネィ卜 (halacrinate), へキサクロロブ夕ジェン0^&(：11101"01) (116116)、へキサコナゾール（116 3(：0 016)、 へキシルチオフォス （hexylthiofos), ハイド口キシキノリンサルフェイト （8- hydroxyquinol ine sulfate), イマザリ Jレ （imazalil)、 イミベンコナゾ一 レ (imibenconazole)、イミノク夕ジン (iminoctadine)、ィプコナソ一レ (ipconazole)、 ィプロベンホス （iprobenfos)、 ィプロジオン （iprodione)、 イソプロチオラン ( isoprothiolane) , ィプロバリカルプ （ iproval icarb )、 イソバレジオン ( isovaledione ) , カスカマイシン ( kasugamycin ) > ク レソ千シムメチル (kresoxim- methyl)、 マンカッパ一 (mancopper), マンゼブ （mancozeb)、 マンネブ (maneb)、 メノヽ。ニピリム (mepanipyrim)、 メプロニリレ mepronil)、 メタラキシル (metalaxyl)、メトコナゾ一ル (metconazole)、メタスルホカルブ (methasulfocarb)、 メチラム （metirain)、 メトミノストロビン （metominostrobin)、 ミクロブ夕ニル (myclobutanil), MTF-753 (試験名）、 メベニル （mebenil)、 メカルビンジド (mecarb inzid) 塩化第二水銀 (mercuric chloride),酸化第二水銀 Oner cur i c ox i de)、 塩化第一水銀 （mercurous chloride), メタラキシルー Mdnetalaxy卜 M)、 メタム (met am), メタロキソロン （metazoxolon)、 メ夕ス Jレフォカルプ (methasul focarb), メスフロキサム （methfuroxam)、 メチルブロマイド （methyl bromide)、 メチルイソ チオシァネイ ト （methyl isothiocyanate) , メチルマーキュリーベンゾエイ ト (methylmercury benzoate)、メチルマーキュリージシアンジアミド (methylmercury dicyandi amide) , メ トラフエノン （metrafenone )、 メ トス レフォバックス(Clotrimazole), Katsuno ヽ0 —aceteate (copper acetate), salt ¾te copper carbonate ^ copper carbonate, basic), τΚcopper hydroxide (copper hydroxide), Ricino ——Naphyulen ^ copper naphthenate), Katsuno ——Oleate (copper oleate), copper sulfate opper sul fate)> copper sulfate, basic, copper zinc chromate> cresol, cresol, kufraneb, cuprobam cuprobam), cyazofamid, cyclafuramid, cycloheximide F, cycloheximide H, cyf lufenamid H, cymoxanil, cypendaxone cypendazole, cyconazole az Sip □ Jini Lily (cyprodini 1), cyprofuram (cyprofuram), dazomet (dazomet), debibisipi (DBCP), debacarb (debacarb), decafentin (Decafent in), dehydroacetic acid (dehydroacetic acid), dichlone (dichlone) Dichlorophen, dichlorozol ine, diclobutrazol, diclofuranide, dichlofluanid, diclomedine, dichloran, dithofencarb, dithofencarb, diethylfenrocarbonate (Diclocymet), difenoconazole, diflumetor im, dimethirimole, dimet homorph, dimoxystrobin> diniconazole ), Giniconazo-le-M (diniconazole— M), dinobuton dinocap, dinocap, dinocap-4, dinocap-6, dinocton, dinocton, dinosulfon, dinoterbon, dinoteramine ι, αί phenyl amine ;, dipyrithione (disulf iram), ditalimfos, dithianon, dithianon, DN0C, dodemorph, dodine, dorazoxolone drazoxolon), edifenphos, epoxiconazole, etaconazole, ethirimol, ethirimol, etridiazole, X-tem (Etem), ethoxyquin, ethilquinone Ethylmercury acetate, ethylencury bromide, methylmercury bromide, methylmercury chloride cury chloride), ethylmercury phosphate famoxadone> fenarimol, fenbuconazole, fenamidone, fendazoslam, fenfuram, fenfuram Xenamide (fenhexamid), phenoxanil (fenoxani 1), fenpiclonil (fenpicloni 1), fenprovidin (fenpropidin), fenpropimorph (fenpropimo 卬 h), fentin (fentin), ferban (ferbam), ferimzone (ferimzone), fluazinam (fluazinam), fluodioxonil, fluoloimide, fluquinconazole, flusilazole, flus Flusulfamide, Flutolanil, Flutriafol, Folpet, Josetyl-aluminum, Foberidazole, Furaxyl, Furametpyr, Furametpyr fenaminosul f), fenapanil (fenapani 1), fenitropan (fenitropan), fenoxanil (fenoxani 1), flumetover (flumetover), flumorph (flumorph), fluotrimazole, fluoxastrobin, fluoxastrobin Pill (fur tpyr), fluconanil (furcarbanil), fluconazole (furconazole), fluconazo-lucis (furconazole-cis), flemeshik tnx uurmecycloxli, furophanate, guazatine, Glyodin, griseofulvin, Hexachlorobenzene, hexaconazole, hexaconazole, hymexazol, zo, halacrinate, hexachlorobutene 0 ^ & (: 11101 "01) (116116) , Hexaconazole (116 3 (: 0 016), Hexylthiofos, Hyd-mouth xyquinoline sulphate (8-hydroxyquinol ine sulfate), Imazari Jre (imazalil), Imibenconazole (imibenconazole), Iminocon evening Gin (iminoctadine), ipconazole (ipconazole), iprobenfos (iprobenfos), iprodione (iprodione), isoprothiolane (isoprothiolane), iproval icarb, isovaledione (ugas) -methyl), mancopper, mancozeb, maneb, maneno. Nipirim (mepanipyrim), mepronilile mepronil), metalaxyl (metalaxyl), metconazole (metconazole), methasulfocarb (methasulfocarb), metiram (metirain), metominostrobin (metominostrobin), microbuinil (myclobutan53), TF (Test name), mebenil, mecarb inzid, mercuric chloride, mercuric oxide Oner curic ox ide, mercurous chloride, metalaxylol M) , Metam, metalazoxolon, methasul focarb, methfuroxam, methyl bromide, methyl isothiocyanate, methyl mercury benzoate (methylmercury benzoate), methylmercury dicyandiamide, metrafenone, methos refobax
(metsulfovax), ミルネブ （milneb)、 ミクロゾリン （myclozolin)、 メトキシメチ ルマーキュリークロライド (2-methoxyethylmercury chloride), ナノ、'ム (nabam), ニ ッ ケ ル ビ ス （ ジ メ チ ル ジ チ ォ カ ー ノ' メ ー ト ） （ nickel bis (dimethyldithiocarbamate) )、 ニ トロタールイソプロ ピル （nitrotha卜 isopropyl)> ヌァリモル （nuarimol)、 ナ夕マイシン （natamycin)、 ニコビフェン(metsulfovax), milneb (milneb), microzolin (myclozolin), methoxymethylmercury chloride (2-methoxyethylmercury chloride), nano, 'nabam', nickel bis (dimethyl methylthiocano) 'Mate) (nickel bis (dimethyldithiocarbamate)), nitrotar isopropyl> nuarimol, nayumycin, nicobifen
(nicobifen)、 ニトロスチレン (ni trostyrene)、 ォクチリノン (octhilinone)、 ォ フレース（ofurace)、ォキサジキシル（oxadixyl)、ォキシカルポキシン（oxycarboxin)、 ォキシポコナゾールフマール酸塩（oxpoconazole fumarate),ォーシーェイチ（0CH)、 ォリサストロビン （Orysastrobin)、 有機銅 （oxine copper)、 ぺフラゾエート pefurzoate)、 ペンコナゾール enconazole)、 ペンシクロン 、pencycuron)、 フ タライド （phthalide)、 ピぺラリン (piperalin), ポリオキシン (polyoxins), 炭 酸水素力リゥム (potassium hydrogen carbonate) , プロべナゾー Jレ (probenazole プロクロラズ（prochloraz)、 プロシミドン （procymidone)、 プロパモカルプ塩酸塩(nicobifen), nitrostyrene, octhilinone, ofurace, oxadixyl, oxacarboxin, oxypoconazole fumarate, oxpoconazole (0CH) ), Orysastrobin, oxine copper, perfurazoate pefurzoate), penconazole enconazole), pencyclon, pencycuron), phthalide, phthalide, piperalin, polyoxins, hydrogen carbonate Potassium hydrogen carbonate, probenazole J (probenazole), procymidone, propamocarp hydrochloride
(.propamocarb hydrochloride), ブロヒコナゾール (propiconazole)、 プロヒ不ブ(.propamocarb hydrochloride), Probiazole, Prohibu
^propineb) , ピラゾホス yrazophos)、 匕リフエノックス (pyrifenox ヒリメ 夕ニル （pyrimethanil)、 ピロキロン （pyroqui Ion)、 ペン夕クロ口フエノール^ propineb), pyrazophos yrazophos), pyrifenox (pyrifenox), pyromethanil, pyroquilon (pyroqui Ion), pen phenol mouth phenol
(.pentachlorophenol (PCP))、 尿素フエニリレフ K銀 (.phenylmercuriurea), フエニリレ マ一キュリーァセティト 、phenylmercury acetate)、 フエニルマ一キユリ一クロラ ィ ド ( phenylmercury chloride )、 フエニ レマ——キユ リ ——ナイ 卜 レイ 卜(.pentachlorophenol (PCP)), urea phenylenecurate K silver (.phenylmercuriurea), phenylenecury acetate, phenylmercury acetate), phenylmercury chloride, phenylmercury chloride, phenylenecury chlorideレ イ レ イ
(phenylmercury nitrate), フエニルマーキュリーサリシレイト (phenylmercury salicylate), フォスジフェン（phosdiphen)、 ピコキシス卜ロビン（picoxystrobin)、 ポリ力ルバメイト (polycarbamate), ポリオクソリム （polyoxor im)、 ポ夕シゥムァ サイド (potassium azide)¾ タシゥムポリサルフアイド (potassium polysulfide), プロキナジド （proquinazid)、 プロチォカルプ （prothiocarb)、 プロチォコナゾ一 ル （prothioconazole)、 ピラカルボリ ド （pyracarbol id)、 ピラクロス卜ロビン(phenylmercury nitrate), phenylalanine Mercury salicylate rate (phenylmercury salicylate), Fosujifen (phosdiphen), Pikokishisu Bok Robin (picoxystrobin), poly force Rubameito (polycarbamate), Poriokusorimu (polyoxor im), Po evening Shiumua side (potassium azide) ¾ Potassium polysulfide, proquinazid, prothiocarb, prothiocarb, prothioconazole, pyracarbol id, pyraclostrobin
(pyraclostrobin),ピリジニ卜リル（pyridini tri 1)、ピロキシクロア（pyroxychlor)、 ピロキシサルファ （pyroxyfur)、 フエニルフエノール （2-phenylphenol)、 キノメチ ォネー ト（quinomethionate)、 キノキシフェン （ quinoxyfen )、 キントゼン quintozene) キナセ卜ール （quinacetol)、 キナザミド （quinazamid)、 キンコナ ゾール（quinconazole)、ラベンザゾ一ル（rabenzazole)、炭酸水素ナトリゥム (sodium hydrogen carbonate)、次亜塩素酸ナトリゥム（sodium hypochlorite)、硫黄（sul fur)、 スピロキサミン （spiroxamine)、 サリチルァニリド （sal icylani 1 ide)、 シルチオフ アム （silthiofam)、 シメコナゾ一ル （simeconazole)、 アジ化ナトリウム （sodium azide)、 ソジゥムォ Jレトフェニリレフエノキサイド （sodium orthophenylphenoxide)、 ソジゥムペンタクロロフエノキサイド （sodium pentachlorophenoxide)、 ソジゥム ポリサルファイド （sodium polysulfide), ストレプトマイシン （streptomycin), テフコナゾ—— レ (tebuconazole)、 テクナセン (tecnazene) , テトラコナゾ、——リレ ( tetraconazole) , チアベンダゾール （thiabendazole) , チアジアジン (thiadiazin/milneb) , チフルザミド （ thi fluzamide)、 チオファネ一トメチル (thiophanate-methyl),チラム (thiram), トルク口ホスメチル（tolclofos- methyl)、 トリルフラニド （tolylfluanid)、 トリアジメホン （triadimefon)、 トリアジメノ一 ル (toriadimenol)、トリァゾキシ F (triazoxide) トリシクラゾール (tricyclazole)、 トリデモルフ （tridemorph)、 トリフルミゾール （trif lumizole：)、 トリホリン (triforine), トリチコナゾ一ル（triticonazole)、テーシーエムテービ一（TCMTB)、 テクロフ夕ラム （tecloftalam)、 テコラム （tecoram)、 チアジフルァ（thiadifluor) チシォフェン （thicyofen)、 チォクロルフェンフィム （thiochlorfenphim)、 チオメ ルサム（thiomersal)、チオファネィト (thiophanate)、チォキノックス (thioquinox)、 チアジニル （tiadinil)、 チォキシミド （tioxymid)、 トリマーキユリアセティト (tolylmercury acetate)、 トリアミフォス (triamiphos),卜リアリ ¾: （triariniol)、 トリァズブチル (triazbutil), トリブチルチンオキサイド (tributyltin oxide), トリクルアミド (trichlamide), トリフロキシストロビン (tri f loxystrobin) , バ リダマイシン （validamycin)、 ビンクロゾリン （vinclozol in)、 硫酸亜鉛（zinc sulfate), ジネブ （zineb)、 ジラム （ziram)、 ゾキサミド (zoxamide), ザリルアミ ド （zarilamid)、 ジンクナフテネイト （zinc naphthenate)、 ゾキサミド (zoxamide) 及びシィ夕ケ菌糸体抽出物。 (pyraclostrobin), pyridinitril (pyridini tri 1), pyroxycycloa (pyroxychlor), pyroxysulfur (pyroxyfur), phenylphenol (2-phenylphenol), quinometi Quinomethionate, quinoxyfen, quintozene, quinacetol, quinazamide, quinazamid, quinconazole, rabenzazole, sodium hydrogen carbonate, next Sodium hypochlorite, sulfur (sul fur), spiroxamine (spiroxamine), salicylanilide (sal icylani 1 ide), silthiofam (silthiofam), simeconazole, sodium azide (sodium azide), sodium azide J Lettophenylelephenoxide (sodium orthophenylphenoxide), sodium pentachlorophenoxide (sodium pentachlorophenoxide), sodium polysulfide (sodium polysulfide), streptomycin (streptomycin), tefconazo——tebuconazole, tecnazenezo, tetranazone , — Lile (tetraconazole), thiabendazole, thiadiazin / milneb, thifluzamide, thi fluzamide, thiophanate-methyl, thiram, tolclofos-methyl, tolylfluanid Triadimefon, triadimefol, toriadimenol, triazoxide F (triazoxide) tricyclazole, tridemorph (tridemorph), triflumizole (trif lumizole :), triforine, triticonazole (tritic) TCMTB, tecloftalam, tecoram, thiazidifluor, thicyofen, thiochlorfenphim, thiomersal, thiophanate, thiophanate thioquinox), Chia Nil (tiadinil), tioxymid (tioxymid), trimarkicuritate (tolylmercury acetate), triamiphos (triamiphos), triaryli ¾: (triariniol), triazbutyl (triazbutil), tributyltin oxide (tributyltin oxide), trichlamide (trichlamide) ), Trifloxystrobin, validamycin, vinclozol in, zinc sulfate (zinc sulfate), zineb, ziramide, zoxamide, zarilamid ), Zinc naphthenate, zoxamide and mycelium extract.
なお、 本願記載のスルファモイル化合物と上記殺菌剤との混合物も良好な殺菌活 性を示す。 In addition, the mixture of the sulfamoyl compound described in the present application and the bactericide also has a good bactericidal activity. Shows sex.
殺菌剤組成物の相乗的殺菌効果については次のように説明することができる。 即 ち、 個々の活性化合物は、 その殺菌活性にそれぞれ欠点を示す場合が多くあるが、 その場合 2種の活性化合物を組合せた殺菌活性が、 その 2種の化合物各々の活性の 単純な合計 （期待される活性） よりも大きくなる場合にこれを相乗作用という。 2 種の殺菌剤の特定組合せにより期待される活性は、 次のように計算することができ る。 （コルビ一 （C o l b y S. R.)> 除草剤の組合せの相乗および括抗作用反 応の計算、 ウィード （We e d)、 第 1 5巻、 2 0〜2 2頁 （1 9 67年） を参照）  The synergistic germicidal effect of the germicidal composition can be explained as follows. That is, the individual active compounds often exhibit their bactericidal activity in each case, but in this case the bactericidal activity of the combination of the two active compounds is simply the sum of the activities of each of the two compounds ( This is referred to as synergism when it is greater than the expected activity). The expected activity of a particular combination of two fungicides can be calculated as follows. (Colby SR> Calculation of synergistic and antagonistic reaction of herbicide combinations, see Weed, Vol. 15, pages 20-22 (1967))
E=a + j3 - ( β/1 0 0) E = a + j3-(β / 1 0 0)
：殺菌剤 Aを a g a i aの量で処理したときの抑制率  ： Inhibition rate when disinfectant A was treated with the amount of ag aia
β ：殺菌剤 Βを b g a i _ h aの量で処理したときの抑制率 β: inhibition rate when bactericide 処理 was treated with the amount of b g a i _ ha
E：殺菌剤 Aを a g a i /h a, 殺菌剤 Bを b g a i Zh aの量で処理した場合に 期待される抑制率 E: Expected inhibition rate when fungicide A is treated with agai / ha and fungicide B with bgaiZha
即ち、 実際の抑制率が上記計算結果 Eより大きいならば組合せによる活性は相乗 作用を示すということができる。  That is, if the actual inhibition rate is larger than the above calculation result E, it can be said that the activity by the combination shows a synergistic effect.
本発明殺菌剤組成物を使用するにあたっては、 通常適当な固体担体又は液体担体 と混合し、 更に所望により界面活性剤、 浸透剤、 展着剤、 増粘剤、 凍結防止剤、 結 合剤、 固結防止剤、 崩壊剤、 消泡剤、 防腐剤および分解防止剤等を添加して、 液剤 When using the bactericide composition of the present invention, it is usually mixed with a suitable solid carrier or liquid carrier, and if necessary, a surfactant, a penetrant, a spreading agent, a thickener, a deicing agent, a binder, Add anti-caking agent, disintegrant, defoamer, preservative, decomposition inhibitor, etc.
^soluble concentrate)、 乳剤 (emulsif iable concentrate)、 7 和剤 (wet table powder), τΚ溶剤 (water soluble powder)、顆粒水和剤 (water dispersible granule)、 顆粒水溶剤 （water soluble granule), 懸濁剤 (suspension concentrate)、 乳獨 剤 (concentrated emulsion), サスボエマルジョン (suspoemulsion)、 マイクロエ マルジヨン （microemulsion)、 粉剤 (dustable powder), 粒剤 (granule) および ゲル剤 （gel) 等任意の剤型の製剤にて実用に供することができる。 また、 省力化お よび安全性向上の観点から、 上記任意の剤型の製剤を、 水溶性カプセルおよび水溶 性フィルムの袋等の水溶性包装体に封入して供することもできる。 ^ soluble concentrate), emulsion (emulsifiable concentrate), 7 wettable powder, τΚ solvent (water soluble powder), water dispersible granule, water soluble granule, suspension Preparation (concentrated emulsion), suspoemulsion (suspoemulsion), microemulsion, dustable powder, granule and gel, etc. It can be put to practical use as a formulation. In addition, from the viewpoint of labor saving and improvement of safety, the preparation of any of the above dosage forms can be provided in a water-soluble package such as a water-soluble capsule or a bag of a water-soluble film.
固体担体としては、 例えば石英、 カオリナイト、 パイロフイライト、 セリサイト、 タルク、 ベントナイト、 酸性白土、 ァタパルジャイト、 ゼォライトおよび珪藻土等 の天然鉱物質類、 炭酸カルシウム、 硫酸アンモニゥム、 硫酸ナトリウムおよび塩化 力リゥム等の無機塩類、 合成シリカならびに合成シリケ一卜が挙げられる。 Examples of solid carriers include quartz, kaolinite, pyrophyllite, sericite, talc, bentonite, acid clay, attapulgite, zeolite, and diatomaceous earth. Natural minerals, inorganic salts such as calcium carbonate, ammonium sulfate, sodium sulfate and chloride chloride, synthetic silica and synthetic silicate.
液体担体としては、 例えばエチレングリコール、 プロピレングリコールおよびィ ソプロパノール等のアルコール類、 キシレン、 アルキルベンゼンおよびアルキルナ フタレン等の芳香族炭化水素類、 プチルセ口ソルブ等のエーテル類、 シクロへキサ ノン等のケトン類、 ァ—プチロラクトン等のエステル類、 N—メチルピロリドンお よび N—ォクチルピロリドン等の酸アミド類、 大豆油、 ナ夕ネ油、 綿実油およびヒ マシ油等の植物油ならびに水が挙げられる。  Examples of the liquid carrier include alcohols such as ethylene glycol, propylene glycol and isopropanol; aromatic hydrocarbons such as xylene, alkylbenzene and alkylnaphthalene; ethers such as butyl sorbate; and ketones such as cyclohexanone. And esters such as N-methylpyrrolidone, acid amides such as N-methylpyrrolidone and N-octylpyrrolidone, vegetable oils such as soybean oil, naney oil, cottonseed oil and castor oil, and water.
これら固体および液体担体は、 単独で用いても 2種以上を併用してもよい。 界面活性剤としては、 例えばポリオキシエチレンアルキルエーテル、 ポリオキシ ェチレンアルキルァリ一ルエーテル、 ポリォキシェチレンスチリルフエニルエーテ ル、 ポリオキシエチレンポリオキシプロピレンブロックコポリマー、 ポリオキシェ チレン脂肪酸エステル、 ソルビタン脂肪酸エステルおよびポリオキシエチレンソル ビ夕ン脂肪酸エステル等のノニオン性界面活性剤、 アルキル硫酸塩、 アルキルベン ゼンスルホン酸塩、 リグニンスルホン酸塩、 アルキルスルホコハク酸塩、 ナフタレ ン; Vレホン酸塩、 アルキルナフタレンスルホン酸塩、 ナフ夕レンスルホン酸のホル マリン縮合物の塩、 アルキルナフタレンスルホン酸のホルマリン縮合物の塩、 ポリ ォキシエチレンアルキルァリールエーテル硫酸および燐酸塩、 ポリオキシエチレン スチリルフェニルエーテル硫酸および燐酸塩、 ポリ力ルポン酸塩およびポリスチレ ンスルホン酸塩等のァニオン性界面活性剤、 アルキルアミン塩およびアルキル 4級 アンモニゥム塩等の力チォン性界面活性剤ならびにァミノ酸型およびべタイン型等 の両性界面活性剤が挙げられる。  These solid and liquid carriers may be used alone or in combination of two or more. Examples of the surfactant include polyoxyethylene alkyl ether, polyoxyethylene alkylaryl ether, polyoxyethylene styrene phenyl ether, polyoxyethylene polyoxypropylene block copolymer, polyoxyethylene fatty acid ester, sorbitan fatty acid ester And nonionic surfactants such as polyoxyethylene sorbin fatty acid esters, alkyl sulfates, alkyl benzene sulfonates, lignin sulfonates, alkyl sulfosuccinates, naphthalenes; V levonates, alkyl naphthalene sulfonic acids Salt, salt of formalin condensate of naphthylene sulfonic acid, salt of formalin condensate of alkyl naphthalene sulfonic acid, polyoxyethylene alkyl aryl ether sulfate and phosphate, poly Xanthic surfactants such as xylethylene styryl phenyl ether sulfate and phosphate, polycarboxylic acid salts and polystyrene sulfonic acid salts; strong surfactants such as alkylamine salts and alkyl quaternary ammonium salts; Examples include amphoteric surfactants such as a tine type.
これら界面活性剤の含有量は、 特に限定されるものではないが、 本発明の製剤 1 0 0重量部に対し、 通常 0 . 0 5〜 2 0重量部の範囲が望ましい。 また、 これら界 面活性剤は、 単独で用いても 2種以上を併用してもよい。 発明を実施するための最良の形態  The content of these surfactants is not particularly limited, but is usually preferably in the range of 0.05 to 20 parts by weight based on 100 parts by weight of the preparation of the present invention. These surfactants may be used alone or in combination of two or more. BEST MODE FOR CARRYING OUT THE INVENTION
次に本発明殺菌剤組成物を用いる場合の製剤の配合例を示す。 但し本発明の配合 例は、 これらのみに限定されるものではない。 なお、 以下の配合例において 「部」 は重量部を意味する。 Next, a formulation example of a preparation when the fungicide composition of the present invention is used will be described. However, the composition examples of the present invention are not limited to these. In the following formulation examples, "parts" Means part by weight.
〔水和剤 (wet table powder)]  [Wettable powder]
本発明殺菌剤組成物 0 1〜80部 Fungicide composition of the present invention 0 1 to 80 parts
固体担体 5 98. 9部 Solid carrier 5 98. 9 parts
界面活性剤 ：！〜 10部 Surfactant :! ~ 10 copies
その他 0〜 5部 Others 0-5 copies
その他として、 例えば固結防止剤、 分解防止剤等が挙げられる ( 〔乳 剤 (emulsif iable concentrate)] Other examples include, for example, an anti-caking agent and an anti-decomposition agent ( [emulsifiable concentrate]).
本発明殺菌剤組成物 0. 1〜30部 Fungicide composition of the present invention 0.1 to 30 parts
液体担体 45〜 95部 Liquid carrier 45 to 95 parts
界面活性剤 4. 9〜： L 5部 Surfactant 4.9-: L 5 parts
その他 0〜10部 Others 0 to 10 copies
その他として、 例えば展着剤、 分解防止剤等が挙げられる。 〔懸獨 (suspension concentrate)]  Other examples include spreading agents, decomposition inhibitors and the like. [Suspension concentrate]
本発明殺菌剤組成物 0. 1〜70部 Fungicide composition of the present invention 0.1 to 70 parts
液体担体 15〜 98. 89部 Liquid carrier 15 ~ 98. 89 parts
界面活性剤 1〜 12部 Surfactant 1-12 parts
その他 0. 01〜 30部 Others 0.01 to 30 copies
その他として、 例えば凍結防止剤、 増粘剤等が挙げられる。 〔顆粒水和剤 (water dispersible granule))  Other examples include an antifreezing agent and a thickener. (Water dispersible granule)
本発明殺菌剤組成物 0. 1〜 90部 Fungicide composition of the present invention 0.1 to 90 parts
固体担体 0〜 98. 9部 Solid carrier 0 to 98.9 parts
界面活性剤 1〜20部 Surfactant 1-20 parts
その他 0〜10部 Others 0 to 10 copies
その他として、 例えば結合剤、 分解防止剤等が挙げられる。 〔液 剤 (soluble concentrate))  Other examples include a binder and a decomposition inhibitor. (Soluble concentrate)
本発明殺菌剤組成物 0. 01〜 70部 The fungicide composition of the present invention 0.01 to 70 parts
液体担体 20〜99. 99部 Liquid carrier 20-99.99 parts
その他 0〜10部 その他として、 例えば凍結防止剤、 展着剤等が挙げられる。 Others 0 to 10 copies Other examples include an antifreezing agent and a spreading agent.
〔粒 剤 （granule)]  [Granule]
本発明殺菌剤組成物 0. 01〜 80部 The fungicide composition of the present invention 0.01 to 80 parts
固体担体 10〜 99. 99部 Solid carrier 10-99.99 parts
その他 0〜： 10部 Others 0-: 10 copies
その他として、 例えば結合剤、 分解防止剤等が挙げられる。  Other examples include a binder and a decomposition inhibitor.
〔粉 剤 (dustable powder)]  [Dustable powder]
本発明殺菌剤組成物 0. 01〜 30部 The fungicide composition of the present invention 0.01 to 30 parts
固体担体 65〜99. 99部 Solid carrier 65-99.99 parts
その他 0〜5部 Others 0-5 copies
その他として、 例えばドリフト防止剤、 分解防止剤等が挙げられる。  Other examples include an anti-drift agent and an anti-decomposition agent.
使用に際しては上記製剤を水で 1〜 10000倍に希釈してまたは希釈せずに、 有効成分が 1ヘクタール （ha) 当たり 0. 0001〜50kg、 好ましくは 0. 00 1 ~ 10 kgになるように散布する。  For use, the above-mentioned preparations are diluted with water 1 to 10,000 times or not, so that the active ingredient becomes 0.0001 to 50 kg, preferably 0.001 to 10 kg per hectare (ha). Spray.
製剤例  Formulation example
次に具体的に本発明殺菌剤組成物を有効成分とする農薬製剤例を示すがこれらの みに限定されるものではない。 なお、 以下の配合例において 「部」 は重量部を意味 する。 また、 HLBはグリフィンの式により求めた値を表す。  Next, specific examples of agrochemical preparations containing the fungicide composition of the present invention as an active ingredient will be specifically described, but the present invention is not limited thereto. In the following formulation examples, “parts” means parts by weight. HLB represents a value obtained by the Griffin equation.
〔配合例 1〕 水和剤 (wettable powder)  [Formulation Example 1] Wettable powder
スルファモイル化合物 4部 Sulfamoyl compound 4 parts
ホルぺット 16部 Hold 16 parts
パイロフイライト 74部 Pyrofilite 74 parts
ソルポール 5039 4部 Solpole 5039 4 parts
(非イオン性界面活性剤とァニオン性界面活性剤との混合物：東邦化学工業 （株） 商品名）  (Mixture of nonionic surfactant and anionic surfactant: trade name of Toho Chemical Industry Co., Ltd.)
カープレックス #80D 2部 Carplex # 80D 2 copies
(合成含水珪酸：塩野義製薬 （株） 商品名）  (Synthetic hydrous silicic acid: Shionogi & Co., Ltd. product name)
以上を均一に混合粉砕して水和剤とする。  The above is uniformly mixed and pulverized to obtain a wettable powder.
〔配合例 2〕 乳 剤 (emulsifiable concentrate) スルファモイル化合物 2部 [Formulation Example 2] Milk (emulsifiable concentrate) Sulfamoyl compound 2 parts
ホルペット 3部 Holpet 3 parts
キシレン 75部 Xylene 75 parts
N—メチルピロリドン 15部  N-methylpyrrolidone 15 parts
ソルポール 2680 5部 Solpol 2680 5 parts
(非イオン性界面活性剤とァニオン性界面活性剤との混合物：東邦化学工業 （株） 商品名）  (Mixture of nonionic surfactant and anionic surfactant: trade name of Toho Chemical Industry Co., Ltd.)
以上を均一に混合して乳剤とする。  The above are uniformly mixed to form an emulsion.
〔配合例 3〕 懸濁剤 (suspension concentrate)  [Formulation Example 3] Suspension concentrate
スルファモイル化合物 5部 Sulfamoyl compound 5 parts
ホルペット 20部 Holpet 20 parts
ァグリゾ一ル S— 7 10 10部 AGRISOL S-7 10 10 parts
(非イオン性界面活性剤：花王 （株） 商品名）  (Nonionic surfactant: Kao Corporation)
ルノックス 1000 C 0. 5部 Lunox 1000 C 0.5 part
(ァニオン性界面活性剤：東邦化学工業 （株） 商品名）  (Anionic surfactant: trade name of Toho Chemical Industry Co., Ltd.)
キサンタンガム 0. 2部 Xanthan gum 0.2 parts
水' 64. 3部 Wed '64. 3 parts
以上を均一に混合した後、 湿式粉砕して懸濁剤とする。  After uniformly mixing the above, wet pulverization is performed to obtain a suspending agent.
〔配合例 4〕 顆粒水和剤 (water dispersible granule)  [Compounding Example 4] Water dispersible granule
スルファモイル化合物 10部 Sulfamoyl compound 10 parts
ホルペット 65部 Holpet 65 parts
ハイテノール NE-15 5部 Hytenol NE-15 5 parts
(ァニオン性界面活性剤：第一工業製薬 （株） 商品名）  (Anionic surfactant: Daiichi Kogyo Pharmaceutical Co., Ltd.)
バニレックス N 10部 Vanillex N 10 parts
(ァニオン性界面活性剤： 日本製紙 （株） 商品名）  (Anionic surfactant: Nippon Paper Industries Co., Ltd.)
カープレックス # 80D 10部 Carplex # 80D 10 copies
(合成含水珪酸：塩野義製薬 （株） 商品名）  (Synthetic hydrous silicic acid: Shionogi & Co., Ltd. product name)
以上を均一に混合粉砕した後、 少量の水を加えて攪拌混合し、 押出式造粒機で造 粒し、 乾燥して顆粒水和剤とする。 〔配合例 5〕 粒 剤 （granule) After uniformly mixing and pulverizing the above, a small amount of water is added, and the mixture is stirred and mixed. The mixture is granulated by an extruder and dried to obtain a wettable powder. [Formulation Example 5] granule
スルファモイル化合物 2部 Sulfamoyl compound 2 parts
ホルペット 3部 Holpet 3 parts
ベントナイト 50部 Bentonite 50 parts
タルク 45部 Talc 45 parts
以上を均一に混合粉砕した後、 少量の水を加えて攪拌混合し、 押出式造粒機で造 粒し、 乾燥して粒剤とする。  After uniformly mixing and pulverizing the above, a small amount of water is added, and the mixture is stirred and mixed.
〔配合例 6〕 粉 剤 (dustable powder)  [Formulation Example 6] Dustable powder
スルファモイル化合物 1. 5部 Sulfamoyl compound 1.5 parts
ホルペット 1. 5部 Holpet 1.5 parts
カープレックス # 80D 0. 5部 Carplex # 80D 0.5 part
(合成含水珪酸：塩野義製薬 （株） 商品名）  (Synthetic hydrous silicic acid: Shionogi & Co., Ltd. product name)
カオリナイト .95部 Kaolinite .95 copies
リン酸ジイソプロピル 1. 5部 1.5 parts of diisopropyl phosphate
以上を均一に混合粉砕して粉剤とする。  The above is uniformly mixed and pulverized to obtain a powder.
〔配合例 7〕 水和剤 （wet table powder)  [Formulation Example 7] Wettable powder
スルファモイル化合物 4部 Sulfamoyl compound 4 parts
ホルペット 16部 Holpet 16 parts
ポリオキシエチレンラウリルエーテル硫酸アンモニゥム塩 （HLB 1 5) Polyoxyethylene lauryl ether sulfate ammonium salt (HLB15)
2. 5部  2.5 copies
カープレックス # 80D 2. 5部 Carplex # 80D 2.5 copies
(合成含水珪酸：塩野義製薬 （株） 商品名）  (Synthetic hydrous silicic acid: Shionogi & Co., Ltd. product name)
バニレックス N 9部 Vanillex N 9 parts
(ァニオン性界面活性剤： 日本製紙 （株） 商品名）  (Anionic surfactant: Nippon Paper Industries Co., Ltd.)
フバサミ Kクレー 66部 Fubasami K clay 66 parts
(固体担体： フバサミクレー （株） 商品名）  (Solid support: Hubasami Clay Co., Ltd.)
以上を均一に混合して水和剤とする。  The above is uniformly mixed to obtain a wettable powder.
〔配合例 8〕 水和剤 (wet table powder)  (Formulation Example 8) Wettable powder (wet table powder)
スルファモイル化合物 2部 ホルペット 20部 Sulfamoyl compound 2 parts Holpet 20 parts
ポリオキシエチレンラウリルエーテル硫酸アンモニゥム塩 （HLB 15) Polyoxyethylene lauryl ether sulfate ammonium salt (HLB 15)
2. 5部  2.5 copies
カープレックス #80D 2. 5部 Carplex # 80D 2.5 copies
(合成含水珪酸：塩野義製薬 （株） 商品名）  (Synthetic hydrous silicic acid: Shionogi & Co., Ltd. product name)
バニレックス N 9部 Vanillex N 9 parts
(ァニオン性界面活性剤： 日本製紙 （株） 商品名）  (Anionic surfactant: Nippon Paper Industries Co., Ltd.)
フバサミ Kクレー 64部 Fubasami K clay 64 parts
(固体担体： フバサミクレー （株） 商品名）  (Solid support: Hubasami Clay Co., Ltd.)
以上を均一に混合して水和剤とする。  The above is uniformly mixed to obtain a wettable powder.
〔配合例 9〕 水和剤 （wet table powder)  [Formulation Example 9] wettable powder (wet table powder)
スルファモイル化合物 8部 Sulfamoyl compound 8 parts
シモキサニル 12部 Simoxanil 12 parts
パイロフイライト 74部 Pyrofilite 74 parts
ソルポール 5039 4部 Solpole 5039 4 parts
(非イオン性界面活性剤とァニオン性界面活性剤との混合物：東邦化学工業 （株） 商品名）  (Mixture of nonionic surfactant and anionic surfactant: trade name of Toho Chemical Industry Co., Ltd.)
カープレックス #80D 2部 Carplex # 80D 2 copies
(合成含水珪酸：塩野義製薬 （株） 商品名）  (Synthetic hydrous silicic acid: Shionogi & Co., Ltd. product name)
以上を均一に混合粉砕して水和剤とする。  The above is uniformly mixed and pulverized to obtain a wettable powder.
〔配合例 10〕 乳 剤 (emulsifiable concentrate)  [Formulation Example 10] Milk (emulsifiable concentrate)
スルファモイル化合物 3部 Sulfamoyl compound 3 parts
シモキサニル 2部 Simoxanil 2 parts
キシレン 75部 Xylene 75 parts
N_メチルピロリドン 15部  N_methylpyrrolidone 15 parts
ソルポール 2680 5部 Solpol 2680 5 parts
(非イオン性界面活性剤とァニオン性界面活性剤との混合物：東邦化学工業 （株） 商品名）  (Mixture of nonionic surfactant and anionic surfactant: trade name of Toho Chemical Industry Co., Ltd.)
以上を均一に混合して乳剤とする。 〔配合例 11〕 懸獨剤 (suspension concentrate) The above are uniformly mixed to form an emulsion. (Compounding Example 11) Suspension concentrate
スルファモイル化合物 15部 Sulfamoyl compound 15 parts
シモキサニル 10部 Simoxanil 10 parts
ァグリゾ一ル S— 710 10部 AGRISOL S-710 10 parts
(非イオン性界面活性剤：花王 （株） 商品名）  (Nonionic surfactant: Kao Corporation)
ルノックス 1000 C 0. 5部 Lunox 1000 C 0.5 part
(ァニオン性界面活性剤：東邦化学工業 （株） 商品名）  (Anionic surfactant: trade name of Toho Chemical Industry Co., Ltd.)
キサンタンガム 0. 2部 Xanthan gum 0.2 parts
水 64. 3部 Water 64. 3 parts
以上を均一に混合した後、 湿式粉砕して懸濁剤とする。  After uniformly mixing the above, wet pulverization is performed to obtain a suspending agent.
〔配合例 12〕 顆粒水和剤 (water dispersible granule)  [Formulation Example 12] water dispersible granule
スルファモイル化合物 35部 Sulfamoyl compound 35 parts
シモキサニル 40部 Simoxanil 40 parts
ハイテノール NE- 15 5部 Hytenol NE-15 15 parts
(ァニオン性界面活性剤：第一工業製薬 （株） 商品名）  (Anionic surfactant: Daiichi Kogyo Pharmaceutical Co., Ltd.)
バニレックス N 10部 Vanillex N 10 parts
(ァニオン性界面活性剤： 日本製紙 （株） 商品名）  (Anionic surfactant: Nippon Paper Industries Co., Ltd.)
カープレックス # 80D 10部 Carplex # 80D 10 copies
(合成含水珪酸：塩野義製薬 （株） 商品名）  (Synthetic hydrous silicic acid: Shionogi & Co., Ltd. product name)
以上を均一に混合粉砕した後、 少量の水を加えて攪拌混合し、 押出式造粒機で造 粒し、 乾燥して顆粒水和剤とする。  After uniformly mixing and grinding the above, a small amount of water is added, and the mixture is stirred and mixed. The mixture is granulated by an extruder and dried to obtain a wettable powder.
〔配合例 13〕 粒 剤 (granule)  (Compounding Example 13) Granule
スルファモイル化合物 2部 Sulfamoyl compound 2 parts
シモキサニル 3部 Simoxanil 3 parts
ベントナイト 50部 Bentonite 50 parts
タルク 45部 Talc 45 parts
以上を均一に混合粉砕した後、 少量の水を加えて攪拌混合し、 押出式造粒機で造 粒し、 乾燥して粒剤とする。  After uniformly mixing and pulverizing the above, a small amount of water is added, and the mixture is stirred and mixed.
〔配合例 14〕 粉 剤 (dust able powder) スルファモイル化合物 1. 5部 [Compounding Example 14] Dust able powder Sulfamoyl compound 1.5 parts
シモキサ二^/ 1. 5部 Simoxa2 ^ / 1.5 parts
力一プレックス #80D 0. 5部 Rikiichi Plex # 80D 0.5 part
(合成含水珪酸：塩野義製薬 （株） 商品名）  (Synthetic hydrous silicic acid: Shionogi & Co., Ltd. product name)
カオリナイト 95部 Kaolinite 95 parts
リン酸ジイソプロピル 1. 5部 1.5 parts of diisopropyl phosphate
以上を均一に混合粉砕して粉剤とする。  The above is uniformly mixed and pulverized to obtain a powder.
〔配合例 15〕 乳 剤 (emulsifiable concentrate)  [Formulation Example 15] Milk (emulsifiable concentrate)
スルファモイル化合物 8部 Sulfamoyl compound 8 parts
シモキサニル 8部 Simoxanil 8 parts
ソルべッソ 200 21部 Solbesso 200 21 parts
(溶剤：ェクソン （株） 商品名）  (Solvent: Exxon Co., Ltd.)
N—メチルピロリドン 52部 N-methylpyrrolidone 52 parts
ソルポール 3005 XL 1 1部 Solpol 3005 XL 1 1 copy
(非イオン性界面活性剤とァニオン性界面活性剤との混合物：東邦化学工業 （株） 商品名）  (Mixture of nonionic surfactant and anionic surfactant: trade name of Toho Chemical Industry Co., Ltd.)
以上を均一に混合して乳剤とする。  The above are uniformly mixed to form an emulsion.
〔配合例 16〕 乳 剤 (emulsifiable concentrate)  [Formulation Example 16] Milk (emulsifiable concentrate)
スルファモイル化合物 8部 Sulfamoyl compound 8 parts
シモキサニル 16部 Simoxanil 16 parts
ソルべッソ 200 20部 Solbesso 200 20 parts
(溶剤：ェクソン （株） 商品名）  (Solvent: Exxon Co., Ltd.)
N—メチルピロリドン 47部 N-methylpyrrolidone 47 parts
ソルポール 3005XL 9部 Solpole 3005XL 9 parts
(非イオン性界面活性剤とァニオン性界面活性剤との混合物：東邦化学工業 （株） 商品名）  (Mixture of nonionic surfactant and anionic surfactant: trade name of Toho Chemical Industry Co., Ltd.)
以上を均一に混合して乳剤とする。  The above are uniformly mixed to form an emulsion.
〔配合例 17〕 水和剤 (wettable powder)  (Formulation Example 17) Wettable powder
スルファモイル化合物 3部 ホセチル 17部 Sulfamoyl compound 3 parts Josetil 17 parts
パイロフイライト 74部 Pyrofilite 74 parts
ソルポール 5039 4部 Solpole 5039 4 parts
(非イオン性界面活性剤とァニオン性界面活性剤との混合物：東邦化学工業 （株） 商品名）  (Mixture of nonionic surfactant and anionic surfactant: trade name of Toho Chemical Industry Co., Ltd.)
カープレックス #80D 2部 Carplex # 80D 2 copies
(合成含水珪酸：塩野義製薬 （株） 商品名）  (Synthetic hydrous silicic acid: Shionogi & Co., Ltd. product name)
以上を均一に混合粉砕して水和剤とする。  The above is uniformly mixed and pulverized to obtain a wettable powder.
〔配合例 18〕 乳 剤 (emulsifiable concentrate)  [Formulation Example 18] Milk (emulsifiable concentrate)
スルファモイル化合物 2部 Sulfamoyl compound 2 parts
ホセチル 3部 Josetil 3 parts
キシレン 75部 Xylene 75 parts
N—メチルピロリドン 15部  N-methylpyrrolidone 15 parts
ソルポール 2680 5部 Solpol 2680 5 parts
(非イオン性界面活性剤とァニオン性界面活性剤との混合物：東邦化学工業 （株） 商品名）  (Mixture of nonionic surfactant and anionic surfactant: trade name of Toho Chemical Industry Co., Ltd.)
以上を均一に混合して乳剤とする。  The above are uniformly mixed to form an emulsion.
〔配合例 19〕 懸獨剤 suspension concentrate)  (Formulation Example 19) suspension concentrate)
スルファモイル化合物 5部 Sulfamoyl compound 5 parts
ホセチル 20部 Josetil 20 parts
ァグリゾール S— 710 10部 Agrizole S—710 10 parts
(非イオン性界面活性剤：花王 （株） 商品名）  (Nonionic surfactant: Kao Corporation)
ルノックス 1000 C 0. 5部 Lunox 1000 C 0.5 part
(ァニオン性界面活性剤：東邦化学工業 （株） 商品名）  (Anionic surfactant: trade name of Toho Chemical Industry Co., Ltd.)
キサンタンガム 0. 2部 Xanthan gum 0.2 parts
水 64. 3部 Water 64. 3 parts
以上を均一に混合した後、 湿式粉枠して懸濁剤とする。  After uniformly mixing the above, a wet powder frame is used as a suspension.
〔配合例 20〕 顆粒水和剤 (water dispersible granule)  [Formulation Example 20] water dispersible granule
スルファモイル化合物 10部 ホセチル 65部 Sulfamoyl compound 10 parts Josetil 65 parts
ハイテノール NE- 15 5部 Hytenol NE-15 15 parts
(ァニオン性界面活性剤：第一工業製薬 （株） 商品名）  (Anionic surfactant: Daiichi Kogyo Pharmaceutical Co., Ltd.)
バニレックス N 10部 Vanillex N 10 parts
(ァニオン性界面活性剤： 日本製紙 （株） 商品名）  (Anionic surfactant: Nippon Paper Industries Co., Ltd.)
カープレックス #80D 10部 Carplex # 80D 10 copies
(合成含水珪酸：塩野義製薬 （株） 商品名）  (Synthetic hydrous silicic acid: Shionogi & Co., Ltd. product name)
以上を均一に混合粉砕した後、 少量の水を加えて攪拌混合し、 押出式造粒機で造 粒し、 乾燥して顆粒水和剤とする。  After uniformly mixing and grinding the above, a small amount of water is added, and the mixture is stirred and mixed. The mixture is granulated by an extruder and dried to obtain a wettable powder.
〔配合例 21〕 粒 剤 （granule)  [Compounding Example 21] granule
スルファモイル化合物 2部 Sulfamoyl compound 2 parts
ホセチル 3部 Josetil 3 parts
ベントナイト 50部 Bentonite 50 parts
タルク 45部 Talc 45 parts
以上を均一に混合粉砕した後、 少量の水を加えて攪拌混合し、 押出式造粒機で造 粒し、 乾燥して粒剤とする。  After uniformly mixing and pulverizing the above, a small amount of water is added, and the mixture is stirred and mixed.
〔配合例 22〕 粉 剤 (dustable powder)  (Formulation Example 22) Dustable powder
スルファモイル化合物 1. 5部 Sulfamoyl compound 1.5 parts
ホセチル 1. 5部 Josetil 1.5 parts
カープレックス #80D 0. 5部 Carplex # 80D 0.5 part
(合成含水珪酸：塩野義製薬 （株） 商品名）  (Synthetic hydrous silicic acid: Shionogi & Co., Ltd. product name)
カオリナイト 95部 Kaolinite 95 parts
リン酸ジイソプロピル 1. 5部 1.5 parts of diisopropyl phosphate
以上を均一に混合粉砕して粉剤とする。  The above is uniformly mixed and pulverized to obtain a powder.
〔配合例 23〕 水和剤 (wet table powder)  (Formulation Example 23) Wettable powder (wet table powder)
スルファモイル化合物 9部 9 parts of sulfamoyl compounds
ホセチル 12部 Josetil 12 parts
ポリオキシエチレンラウリルエーテル硫酸アンモニゥム塩 （HLB 15) Polyoxyethylene lauryl ether sulfate ammonium salt (HLB 15)
2. 5部 カープレックス #80D 2. 5部 2.5 copies Carplex # 80D 2.5 copies
(合成含水珪酸：塩野義製薬 （株） 商品名）  (Synthetic hydrous silicic acid: Shionogi & Co., Ltd. product name)
バニレックス N 3部 Vanillex N 3 parts
(ァニオン性界面活性剤： 日本製紙 （株） 商品名）  (Anionic surfactant: Nippon Paper Industries Co., Ltd.)
フバサミ Kクレー 71部 Fubasami K clay 71 parts
(固体担体： フバサミクレー （'株） 商品名）  (Solid support: Hubasami clay ('Co., Ltd.) trade name)
以上を均一に混合して水和剤とする。  The above is uniformly mixed to obtain a wettable powder.
〔配合例 24〕 水和剤 (wettable powder)  (Formulation Example 24) Wettable powder
スルファモイル化合物 1部 1 part sulfamoyl compound
ホセチル 20部 Josetil 20 parts
ポリオキシエチレンラウリルエーテル硫酸アンモニゥム塩 （HLB 15) Polyoxyethylene lauryl ether sulfate ammonium salt (HLB 15)
2. 5部  2.5 copies
カープレックス #80D 2. 5部 Carplex # 80D 2.5 copies
(合成含水珪酸：塩野義製薬 （株） 商品名）  (Synthetic hydrous silicic acid: Shionogi & Co., Ltd. product name)
バニレックス N 3部 Vanillex N 3 parts
(ァニオン性界面活性剤： 日本製紙 （株） 商品名）  (Anionic surfactant: Nippon Paper Industries Co., Ltd.)
フバサミ Kクレー 71部 Fubasami K clay 71 parts
(固体担体： フバサミクレー （株） 商品名）  (Solid support: Hubasami Clay Co., Ltd.)
以上を均一に混合して水和剤とする。  The above is uniformly mixed to obtain a wettable powder.
〔配合例 25〕 水和剤 （wettable powder)  [Formulation Example 25] Wettable powder
スルファモイル化合物 4部 Sulfamoyl compound 4 parts
マンゼブ 16部 Manzeb 16 parts
パイロフイライト 74部 Pyrofilite 74 parts
ソルポール 5039 4部 Solpole 5039 4 parts
(非イオン性界面活性剤とァニオン性界面活性剤との混合物：東邦化学工業 （株) 商品名）  (Mixture of nonionic surfactant and anionic surfactant: trade name of Toho Chemical Industry Co., Ltd.)
カープレックス #80D 2部 Carplex # 80D 2 copies
(合成含水珪酸：塩野義製薬 （株） 商品名）  (Synthetic hydrous silicic acid: Shionogi & Co., Ltd. product name)
以上を均一に混合粉枠して水和剤とする。 〔配合例 26〕 乳 剤 (emulsifiable concentrate) The above is uniformly mixed to form a wettable powder. [Formulation Example 26] Milk (emulsifiable concentrate)
スルファモイル化合物 1部 1 part sulfamoyl compound
マンゼブ 4部 Manzeb 4
キシレン 75部 Xylene 75 parts
N—メチルピロリドン 15部  N-methylpyrrolidone 15 parts
ソルポール 2680 5部 Solpol 2680 5 parts
(非イオン性界面活性剤とァニオン性界面活性剤との混合物：東邦化学工業 （株） 商品名）  (Mixture of nonionic surfactant and anionic surfactant: trade name of Toho Chemical Industry Co., Ltd.)
以上を均一に混合して乳剤とする。  The above are uniformly mixed to form an emulsion.
〔配合例 27J 懸獨剤 (.suspension concentrate)  (Formulation 27J Suspension concentrate)
スルファモイル化合物 5部 Sulfamoyl compound 5 parts
マンゼブ 20部 Manzeb 20 parts
ァグリゾ一ル S—710 10部 AGRISOL S-710 10 parts
(非イオン性界面活性剤：花王 （株） 商品名）  (Nonionic surfactant: Kao Corporation)
ルノックス 1000 C 0. 5部 Lunox 1000 C 0.5 part
(ァニオン性界面活性剤：東邦化学工業 （株） 商品名）  (Anionic surfactant: trade name of Toho Chemical Industry Co., Ltd.)
キサンタンガム 0. 2部 Xanthan gum 0.2 parts
水 64. 3部 Water 64. 3 parts
以上を均一に混合した後、 湿式粉砕して懸濁剤とする。  After uniformly mixing the above, wet pulverization is performed to obtain a suspending agent.
〔配合例 28〕 顆粒水和剤 (water dispersible granule)  [Compounding Example 28] Water dispersible granule
スルファモイル化合物 10部 Sulfamoyl compound 10 parts
マンゼブ 65部 Manzeb 65 parts
ハイテノール NE-15 5部 Hytenol NE-15 5 parts
(ァニオン性界面活性剤：第一工業製薬 （株） 商品名）  (Anionic surfactant: Daiichi Kogyo Pharmaceutical Co., Ltd.)
バニレックス N 10部 Vanillex N 10 parts
(ァニオン性界面活性剤： 日本製紙 （株） 商品名）  (Anionic surfactant: Nippon Paper Industries Co., Ltd.)
カープレックス # 80 D 10部 Carplex # 80 D 10 copies
(合成含水珪酸：塩野義製薬 （株） 商品名）  (Synthetic hydrous silicic acid: Shionogi & Co., Ltd. product name)
以上を均一に混合粉砕した後、 少量の水を加えて攪拌混合し、 押出式造粒機で造 粒し、 乾燥して顆粒水和剤とする。 After uniformly mixing and pulverizing the above, a small amount of water is added, and the mixture is stirred and mixed. Granulate and dry to form a wettable powder.
〔配合例 29〕 粒 剤 （granule)  [Compounding Example 29] Granule
スルファモイル化合物 2部 Sulfamoyl compound 2 parts
マンゼブ 3部 Manzeb 3
ベン卜ナイ卜 50部 Vento Night 50 copies
タルク 45部 Talc 45 parts
以上を均一に混合粉砕した後、 少量の水を加えて攪拌混合し、 押出式造粒機で造 粒し、 乾燥して粒剤とする。  After uniformly mixing and pulverizing the above, a small amount of water is added, and the mixture is stirred and mixed.
〔配合例 30〕 粉 剤 (dustable powder)  (Formulation 30) Dustable powder
スルファモイル化合物 1. 5部 Sulfamoyl compound 1.5 parts
マンゼブ 1. 5部 Manzeb 1.5 parts
カープレックス # 80D 0. 5部 Carplex # 80D 0.5 part
(合成含水珪酸：塩野義製薬 （株） 商品名）  (Synthetic hydrous silicic acid: Shionogi & Co., Ltd. product name)
カオリナイト 95部 Kaolinite 95 parts
リン酸ジイソプロピル 1. 5部 1.5 parts of diisopropyl phosphate
以上を均一に混合粉砕して粉剤とする。  The above is uniformly mixed and pulverized to obtain a powder.
〔配合例 3 1〕 水和剤 (wettable powder)  [Compounding Example 3 1] Wettable powder
スルファモイル化合物 9部 9 parts of sulfamoyl compounds
マンゼブ 12部 Manzeb 12 parts
ポリオキシエチレンラウリルエーテル硫酸アンモニゥム塩 （HLB 1 5) Polyoxyethylene lauryl ether sulfate ammonium salt (HLB15)
2. 5部  2.5 copies
カープレックス # 80D 2. 5部 Carplex # 80D 2.5 copies
(合成含水珪酸：塩野義製薬 （株） 商品名）  (Synthetic hydrous silicic acid: Shionogi & Co., Ltd. product name)
バニレックス N 3部 Vanillex N 3 parts
(ァニオン性界面活性剤： 日本製紙 （株） 商品名）  (Anionic surfactant: Nippon Paper Industries Co., Ltd.)
フバサミ Kクレー 7 1部 Fubasami K Clay 7 1 copy
(固体担体： フバサミクレー （株） 商品名）  (Solid support: Hubasami Clay Co., Ltd.)
以上を均一に混合して水和剤とする。  The above is uniformly mixed to obtain a wettable powder.
〔配合例 32〕 水和剤 (wettable powder) スルファモイル化合物 1部 (Formulation Example 32) Wettable powder 1 part sulfamoyl compound
マンゼブ 15部 Manzeb 15 parts
ポリオキシエチレンラウリルエーテル硫酸アンモニゥム塩 （HLB 15) Polyoxyethylene lauryl ether sulfate ammonium salt (HLB 15)
2. 5部  2.5 copies
カープレックス # 80D 2. 5部 Carplex # 80D 2.5 copies
(合成含水珪酸：塩野義製薬 （株） 商品名）  (Synthetic hydrous silicic acid: Shionogi & Co., Ltd. product name)
バニレックス N 3部 Vanillex N 3 parts
(ァニオン性界面活性剤： 日本製紙 （株） 商品名）  (Anionic surfactant: Nippon Paper Industries Co., Ltd.)
フバサミ Kクレー 76部 Fubasami K clay 76 parts
(固体担体： フバサミクレー （株） 商品名）  (Solid support: Hubasami Clay Co., Ltd.)
以上を均一に混合して水和剤とする。 本発明組成物の有用性について、以下の試験例において具体的に説明する。但し、 本発明組成物はこれらのみに制限されるものではない。  The above is uniformly mixed to obtain a wettable powder. The usefulness of the composition of the present invention will be specifically described in the following test examples. However, the composition of the present invention is not limited only to these.
〔試験例〕  (Test example)
試験例 1 ブドウべと病防除効果試験 Test example 1 Grape downy mildew control effect test
直径 7 cmのポットで育成した 3〜4葉期のブドウ （品種：力ベルネ） に、 ブド ウベと病菌 （Plasmopara viticola) の胞子懸濁液 （ 2 X 10 J個/ m 1 ) を噴霧 し、 温度 20 ：、 湿度 95%以上の接種箱に 2日間入れた。 風乾後、 配合例 7に準 じて調製した本発明殺菌剤組成物の製剤を水で希釈することにより各薬量になるよ うに調製した薬液をスプレーガンを用いポット当たり 10m l散布した。 Spray a spore suspension (2 x 10 J / m 1) of vine and Plasmopara viticola onto grape at the 3-4 leaf stage (cultivar: Riki Vernet) grown in a pot with a diameter of 7 cm. Temperature 20: placed in an inoculation box with a humidity of 95% or more for 2 days. After air-drying, a solution of the bactericide composition of the present invention prepared according to Formulation Example 7 was diluted with water, and a chemical solution prepared to each dosage was sprayed using a spray gun to spray 10 ml per pot.
その後、 温室におき、 接種 10日後に形成された病斑面積の接種葉に占める割合 を測定し、 下記の式に従い、 防除価を算出した。 防除価 = 〔1一 （処理区病斑面積率/無処理区病斑面積率)〕 X I 00 その結果を第 1表に示す。 試験例 2 ブドウべと病防除効果試験  After that, the plants were placed in a greenhouse, the ratio of the lesion area formed 10 days after the inoculation to the inoculated leaves was measured, and the control value was calculated according to the following formula. Control value = [11 (area ratio of treated spot / area ratio of untreated section)] XI 00 The results are shown in Table 1. Test example 2 Grape downy mildew control effect test
配合例 15に準じて調製した製剤を用いて、試験例 1の試験方法に準じて試 験を行った。 結果を第 2表に示す。 Using the preparation prepared according to Formulation Example 15, test according to the test method of Test Example 1. Test was carried out. The results are shown in Table 2.
試験例 3 ブドウべと病防除効果試験 Test example 3 Grape downy mildew control effect test
配合例 23に準じて調製した製剤を用いて、試験例 1の試験方法に準じて試 験を行った。 結果を第 3表に示す。 試験例 4 バレイショ疫病防除効果試験  A test was conducted according to the test method of Test Example 1 using the preparation prepared according to Formulation Example 23. Table 3 shows the results. Test example 4 Potato disease control effect test
直径 7 cmのポットで育成したバレイショ （品種：ダンシャク） に、 配合例 8に 準じて調製した本発明殺菌剤組成物の製剤を水で希釈することにより各薬量になる ように調製した薬液をスプレーガンを用いポット当たり 10ml散布した。 10日 間ガラス温室で生育した後、 ジャガイモ疫病菌 （Phytophthora infestans) の胞子 懸濁液 （2X 105個 ml) を噴霧し、 温度 20°C、 湿度 95 %以上の接種箱に 入れた。 5日後に形成された病斑面積の接種葉に占める割合を測定し、 試験例 1の 式と尚じ式に従い、 防除価を算出した。 A potato (cultivar: Danshak) grown in a pot with a diameter of 7 cm was diluted with water to prepare a solution of the fungicidal composition of the present invention prepared according to Formulation Example 8 so that each drug solution was prepared to have a respective dose. Using a spray gun, 10 ml was sprayed per pot. After growing in a glass greenhouse for 10 days, a spore suspension (2 × 10 5 ml) of potato blight fungus (Phytophthora infestans) was sprayed and placed in an inoculation box at a temperature of 20 ° C and a humidity of 95% or more. The ratio of the area of the lesion formed after 5 days to the inoculated leaves was measured, and the control value was calculated according to the formula in Test Example 1 and the same formula.
その結果を第 4表に示す。 試験例 5 バレイショ疫病防除効果試験  Table 4 shows the results. Test Example 5 Potato Blight Control Effect Test
配合例 24に準じて調製した製剤を用いて、試験例 4の試験方法に準じて試 験を行った。 結果を第 5表に示す。 試験例 6 バレイショ疫病防除効果試験  A test was performed according to the test method of Test Example 4 using the preparation prepared according to Formulation Example 24. Table 5 shows the results. Test Example 6 Test for controlling potato blight
配合例 32に準じて調製した製剤を用いて、試験例 4の試験方法に準じて試 験を行った。 結果を第 6表に示す。 試験例 7 バレイショ疫病防除効果試験  The test was performed according to the test method of Test Example 4 using the preparation prepared according to Formulation Example 32. The results are shown in Table 6. Test Example 7 Test for controlling potato blight
直径 15 cmのポットで育成したバレイショ （品種：ダンシャク） に、 ジャガイ モ疫病菌 （Phytophthora infestans) の胞子懸濁液 （2 10 個 1111 ) を噴霧 し、 温度 20 、 湿度 95%以上の接種箱に 6時間入れた。 風乾後、 配合例 16に 準じて調製した本発明殺菌剤組成物の製剤を水で希釈して各濃度に調製した薬液を スプレーガンを用いポット当たり 10m 1散布した。 その後、再び加湿条件におき、接種 5日後に形成された病斑面積の接種葉に占める 割合を測定し、 試験例 1の式と同じ式に従い、 防除価を算出した。 Potatoes (variety: Danshak) grown in pots with a diameter of 15 cm are sprayed with a spore suspension of potato blight (Phytophthora infestans) (211, 1111). I put in for 6 hours. After air-drying, the formulation of the bactericide composition of the present invention prepared according to Formulation Example 16 was diluted with water, and a chemical solution adjusted to each concentration was sprayed at 10 ml per pot using a spray gun. Thereafter, the cells were placed again under humidification conditions, the ratio of the lesion area formed 5 days after the inoculation to the inoculated leaves was measured, and the control value was calculated according to the same formula as that of Test Example 1.
その結果を第 7表に示す。 なお、 表中、 Eはコルビーの式における期待値を表す。 〔第 1表〕 薬剤 薬量 ^gai/ha) 防除価 E  Table 7 shows the results. In the table, E represents the expected value in Colby's equation. (Table 1) Drug Drug dosage ^ gai / ha) Control value E
スルファモイル化合物 +ホルぺット 50+200 100 89 Sulfamoyl compound + Holt 50 + 200 100 89
スルファモイル化合物 50 80 Sulfamoyl compound 50 80
ホルぺット 200 45 Hold 200 45
〔第 2表〕 薬剤 薬重 (gai/ha) 防除価 E [Table 2] Drug Weight (gai / ha) Control value E
スルファモイル化合物 +シモキサニル 10 + 10 100 70 スルファモイル化合物 10 50 Sulfamoyl compound + cimoxanil 10 + 10 100 70 Sulfamoyl compound 10 50
シモキサニル 10 40 Simoxanil 10 40
薬剤 薬量 (.gai/ha) 防除価 E Drug Dose (.gai / ha) Control value E
スルファモイル化合物 +ホセチル 75+ 100 100 68 スルファモイル化合物 75 60 Sulfamoyl compound + fosetyl 75+ 100 100 68 Sulfamoyl compound 75 60
ホセチル 100 20 Josetyl 100 20
薬剤 薬量 (gai/ha) 防除価 E 一 スルファモイル化合物 +ホルぺット 100+ 1000 90 85 スルファモイル化合物 100 50 Drug Dosage (gai / ha) Control value E-Sulfamoyl compound + Holt 100+ 1000 90 85 Sulfamoyl compound 100 50
ホルぺット 1000 70 〔第 5表〕 薬剤 薬量 (gai/ha) 防除価 E Hold 1000 70 [Table 5] Drugs Dose (gai / ha) Control value E
スルファモイル化合物 +ホセチル 50+ 1000 92 36 スルファモイル化合物 50 5 Sulfamoyl compound + fosetyl 50+ 1000 92 36 Sulfamoyl compound 50 5
ホセチル 1000 33 Josetil 1000 33
薬剤 薬量 (gai/ha) 防除価 E スルファモイル化合物 +マンゼブ 100+ 1500 91 85 スルファモイル化合物 100 67 Drug Dose (gai / ha) Control value E Sulfamoyl compound + Manzeb 100+ 1500 91 85 Sulfamoyl compound 100 67
マンゼブ 1500 55 Manzeb 1500 55
薬剤 濃度（gai/ha) 防除価 E Drug concentration (gai / ha) Control value E
スルファモイル化合物 +シモキサ.ニル 75+ 150 97 76 スルファモイル化合物 75 5 Sulfamoyl compound + Simoxa.nil 75+ 150 97 76 Sulfamoyl compound 75 5
シモキサニル 150 75 本発明組成物は優れた相乗的殺菌効果を示し、 有用作物に対する薬害も認められ ないため、 農園芸用殺菌剤として有用である。 Simoxanil 150 75 The composition of the present invention exhibits an excellent synergistic bactericidal effect and shows no phytotoxicity to useful crops, and is therefore useful as an agricultural and horticultural fungicide.

Claims

請求の範囲 The scope of the claims
1 . 式 （1 ) ：1. Equation (1):
Figure imgf000032_0001
2
Figure imgf000032_0001
Two
で表される卜 (N, N-ジメチルスルファモイル） -3- 〔2-メチル -3-ブロム- 6-フル ォロインドール- 1-ィル〕 スルホニル -1 , 2, 4-トリァゾールとシモキサニルとを有 効成分として含有することを特徴とする殺菌剤組成物。 (N, N-dimethylsulfamoyl) -3- [2-methyl-3-bromo-6-fluoroindole-1-yl] sulfonyl-1,2,4-triazole and simoxanil A fungicide composition characterized by containing as an active ingredient.
2 . 式 （1 ) で表される卜 （N, N-ジメチルスルファモイル） -3- 〔2-メチル -3 -ブロム- 6-フルォロインドール-卜ィル〕 スルホニル -1 , 2, 4-トリァゾールとホ セチルとを有効成分として含有することを特徴とする殺菌剤組成物。  2. Tri (N, N-dimethylsulfamoyl) -3- [2-methyl-3-bromo-6-fluoroindole-triyl] sulfonyl-1,2,2 represented by the formula (1) A fungicidal composition comprising 4-triazole and fosetyl as active ingredients.
3 . 式 （1 ) で表される 1- (N, N-ジメチルスルファモイル） -3- 〔2-メチル -3-ブロム- 6-フルォロインドール-卜ィル〕 スルホニル- 1， 2, 4-トリァゾ一ルとマ ンゼブとを有効成分として含有することを特徴とする殺菌剤組成物。  3. 1- (N, N-dimethylsulfamoyl) -3- [2-methyl-3-bromo-6-fluoroindole-tolyl] sulfonyl-1,2 represented by the formula (1) A fungicidal composition comprising 4-triazole and manzeb as active ingredients.
4. 式 （1 ) で表される卜 (N, N-ジメチルスルファモイル） -3- 〔2-メチル -3-ブロム- 6-フルォロインドール- 1-ィル〕 スルホニル -1， 2, 4-トリァゾールとホ ルぺットとを有効成分として含有することを特徴とする殺菌剤組成物。  4. Tri (N, N-dimethylsulfamoyl) -3- [2-methyl-3-bromo-6-fluoroindole-1-yl] sulfonyl-1,2 represented by the formula (1) A fungicidal composition comprising, as active ingredients, 4-triazole and potassium.
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