CN1331799C - Concrete pump and preparation method thereof - Google Patents

Concrete pump and preparation method thereof Download PDF

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Publication number
CN1331799C
CN1331799C CNB2006100542424A CN200610054242A CN1331799C CN 1331799 C CN1331799 C CN 1331799C CN B2006100542424 A CNB2006100542424 A CN B2006100542424A CN 200610054242 A CN200610054242 A CN 200610054242A CN 1331799 C CN1331799 C CN 1331799C
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China
Prior art keywords
concrete pumping
agent
sodium
pumping agent
preparation
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Expired - Fee Related
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CNB2006100542424A
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CN1844020A (en
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蒋德双
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Publication of CN1331799C publication Critical patent/CN1331799C/en
Expired - Fee Related legal-status Critical Current
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Abstract

The present invention relates to a technology for a concrete pumping agent. The existing concrete pumping agent is prepared from a single component water reducing agent and a retardation agent and has the defects of poor cement adaptation, poor fluidity, crystal separation under low temperature in winter, pipeline blockage caused by precipitation, abnormal use, extremely instable quality and rapid slump constant loss, and the present invention provides a concrete pumping agent compounded by a multiple water reducing agent and a multi-component retardation component and a preparation method thereof. The concrete pumping agent has the technical scheme that the concrete pumping agent comprises the compositions in weight ratio: 15 to 73 of naphthalenesulfonic acid formaldehyde condensation product, 8 to 50 of sulfamate, 20 to 50 of fatty group hydroxy sulphonate, 0.2 to 0.7 of sodium dodecylbenzene sulfonate, 0 to 1.5 of sodium tripolyphosphate, 0 to 1.5 of sodium hexametaphosphate, 0 to 2 of sucrose and 10 to 20 of water. The concrete pumping agent has the preparation method that the water is added in a reaction kettle to be heated according to the weight ratio, the sodium tripolyphosphate, the sucrose, the sodium hexametaphosphate and the sodium dodecylbenzene sulfonate are orderly added to be stirred, the naphthalenesulfonic acid formaldehyde condensation product, the sulfamate and the fatty group hydroxy sulphonate are stirred and cooled to 23(+/-)3 DEG C, and the concrete pumping agent is obtained.

Description

Concrete pump-feed agent and preparation method
One, technical field
The present invention relates to a kind of concrete technology, especially a kind of concrete pump-feed agent and preparation method.
Two, background technology
At present used concrete is generally provided by large-scale stirring station in construction work, help the control of quality and enhance productivity, labour intensity is low, the duration is short, noise is low, airborne dust is few, be beneficial to advantage such as environmental protection.General concrete all adopts the technology of pumping to pour into a mould at the construction field (site), therefore need concrete to have good flowability and pumpability, but because the concrete of stirring station is to be transported to the working-yard by truck mixer from stirring station, in case traffic jam or road are far away, mobile heavy losses can take place and can't pumping in the overlong time of the concrete that stirs experience.At present the aqua concrete pump-feed agent of selling on the market adopts single-component water reducer and retardant formulated more, thereby there is a following shortcoming: inferior suitability, usually can only adapt to the minority cement type, mobile bad, (composition is Na to separate out crystal under the winter low temperature condition 2SO 4Or CaSO 4), precipitation, cause line clogging, can't normally use, simultaneously, quality is extremely unstable, slump-loss is fast.At number of patent application is 200410016574.4, discloses " a kind of control slump-loss type high performance concrete pumping agent " patented technology, adopts the single-component water reducer, still exists above-mentioned weak point.
Three, summary of the invention
The purpose of this invention is to provide and a kind ofly can even more normally under the low temperature use non-crystallizablely, can adapt to 90% above cement type at 0 ℃, good fluidity, cost is low, polynary water reducer and many components slow setting composition compound concrete pump-feed agent and preparation method.
The technical scheme that purpose of the present invention is taked is to be made up of following constituent and weight ratio:
Concentration is 38% naphthalene sulfonic acidformaldehyde condensation product 15-73
Concentration is 38% sulfamate 8-50
Concentration is 30% aliphatic hydroxyl sulphonate 20-50
Sodium dodecylbenzene sulfonate 0.2-0.7
Tripoly phosphate sodium STPP 0-1.5
Sodium hexametaphosphate 0-1.5
Sucrose 0-2
Water 10-20
Preparation method of the present invention is as follows:
By weight water is added in the reactor, be warmed up to 50 ℃-70 ℃, add tripoly phosphate sodium STPP, sucrose, sodium hexametaphosphate and Sodium dodecylbenzene sulfonate successively, stir 30-40min, after material is dissolved fully, add naphthalene sulfonic acidformaldehyde condensation product, sulfamate, aliphatic hydroxyl sulphonate again, behind the stirring 15-25min, cool to 23 ± 3 ℃, promptly get concrete pump-feed agent.
Naphthalenesulfonate formaldehyde condensation compound water reducer used in the present invention, sulfamate water reducer, aliphatic hydroxyl sulphonate water reducer are high efficiency water reducing agent, belong to anion surfactant, and its effect is to disperse cement granules.Sodium dodecylbenzene sulfonate is an air entrapment agent, is mainly used in to reduce concrete pumping resistance, prevents concrete water bleeding, segregation, improves impervious, freezing and thawing performance simultaneously.Tripoly phosphate sodium STPP, sodium hexametaphosphate, sucrose are retardant, regulate concrete coagulating time.
Starting material used herein are easy to get, and cost is low, effectively improve concrete pumping and keep mobile, pumpability in the long period.Be widely used in structures such as commodity ready-mixed concrete, mass concrete, Steel Concrete, light aggregate concrete, bridge, building, water conservancy project and road surface.
Four, embodiment
Further specify the present invention below in conjunction with embodiment.
Fetch water by weight and 13.8 add in the reactors, after being warming up to 60 ℃, add tripoly phosphate sodium STPP 0.25, sucrose 0.15, sodium hexametaphosphate 0.3 and Sodium dodecylbenzene sulfonate 0.5 successively, stir 30min, after material is dissolved fully, add concentration again and be 38% naphthalene sulfonic acidformaldehyde condensation product 25, concentration and be 38% sulfamate 20, concentration and be 30% aliphatic hydroxyl sulphonate 40, stir 15min after, cool to 23 ℃, promptly obtain concrete pump-feed agent.
Concrete pump-feed agent is delivered to the check of Chongqing City construction project quality test test center, check conclusion: this product is checked by examining concrete performance among " concrete pump-feed agent " JC473-2001, satisfies the requirement of acceptable end product performance index.

Claims (2)

1, a kind of concrete pump-feed agent is characterized in that being made up of following component and weight ratio:
Concentration is 38% naphthalene sulfonic acidformaldehyde condensation product 15-73
Concentration is 38% sulfamate 8-50
Concentration is 30% aliphatic hydroxyl sulphonate 20-50
Sodium dodecylbenzene sulfonate 0.2-0.7
Tripoly phosphate sodium STPP 0-1.5
Sodium hexametaphosphate 0-1.5
Sucrose 0-2
Water 10-20.
2, a kind of concrete pump-feed agent preparation method according to claim 1, it is characterized in that the preparation method is as follows: by weight water is added in the reactor, be warmed up to 50 ℃-70 ℃, add tripoly phosphate sodium STPP, sucrose, sodium hexametaphosphate and Sodium dodecylbenzene sulfonate successively, stir 30-40min, material is dissolved fully after, add naphthalene sulfonic acidformaldehyde condensation product, sulfamate, aliphatic hydroxyl sulphonate again, after stirring 15-25min, cool to 23 ± 3 ℃, promptly get concrete pump-feed agent.
CNB2006100542424A 2006-04-24 2006-04-24 Concrete pump and preparation method thereof Expired - Fee Related CN1331799C (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CNB2006100542424A CN1331799C (en) 2006-04-24 2006-04-24 Concrete pump and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CNB2006100542424A CN1331799C (en) 2006-04-24 2006-04-24 Concrete pump and preparation method thereof

Publications (2)

Publication Number Publication Date
CN1844020A CN1844020A (en) 2006-10-11
CN1331799C true CN1331799C (en) 2007-08-15

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Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101134346B (en) * 2007-08-31 2010-05-19 武汉理工大学 Method of producing pump-transporting light aggregate concrete
CN101143771B (en) * 2007-08-31 2010-05-19 武汉理工大学 Light aggregate concrete pumping agent
CN101948262A (en) * 2010-09-09 2011-01-19 镇江市鑫塔混凝土外加剂有限公司 Efficient pumping aid
CN101987784A (en) * 2010-09-10 2011-03-23 重庆达华砼外加剂科技发展有限公司 Concrete delayed coagulation air entraining agent
CN103342497B (en) * 2013-06-24 2014-11-26 安徽省建筑科学研究设计院 Quick-acting anti-slump restorer for pump concrete
CN105130262A (en) * 2015-08-25 2015-12-09 建华建材(蚌埠)有限公司 Concrete non-toxic pumping agent and preparation method therefor
CN109053018A (en) * 2018-09-20 2018-12-21 贵州凯襄新材料有限公司 A kind of feeding type concrete pump-feed agent and preparation method thereof

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1117031A (en) * 1995-02-11 1996-02-21 卢璋 Pumping agent for non-alkali high-strength concrete
CN1061328C (en) * 1997-03-18 2001-01-31 沈阳建筑工程学院 Production of composite concrete additives from superfined flyash
CN1108281C (en) * 2000-07-20 2003-05-14 上海世强科技有限责任公司 High-performance concrete pumping agent and its prepn process
CN1548395A (en) * 2003-05-21 2004-11-24 上海恒福科技发展有限公司 Concrete pumping aid
CN1181005C (en) * 2001-11-10 2004-12-22 李乃珍 Low slump loss concrete pumping agent
CN1559964A (en) * 2004-02-26 2005-01-05 同济大学 High performance concrete pumping agent controlling falling degree loss type

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1117031A (en) * 1995-02-11 1996-02-21 卢璋 Pumping agent for non-alkali high-strength concrete
CN1061328C (en) * 1997-03-18 2001-01-31 沈阳建筑工程学院 Production of composite concrete additives from superfined flyash
CN1108281C (en) * 2000-07-20 2003-05-14 上海世强科技有限责任公司 High-performance concrete pumping agent and its prepn process
CN1181005C (en) * 2001-11-10 2004-12-22 李乃珍 Low slump loss concrete pumping agent
CN1548395A (en) * 2003-05-21 2004-11-24 上海恒福科技发展有限公司 Concrete pumping aid
CN1559964A (en) * 2004-02-26 2005-01-05 同济大学 High performance concrete pumping agent controlling falling degree loss type

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C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
EE01 Entry into force of recordation of patent licensing contract

Assignee: Chongqing Dahua Concrete Additive Technology Development Co., Ltd.

Assignor: Jiang Deshuang

Contract record no.: 2010500000052

Denomination of invention: Concrete pump and preparation method thereof

Granted publication date: 20070815

License type: Exclusive License

Open date: 20061011

Record date: 20100913

CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20070815

Termination date: 20150424

EXPY Termination of patent right or utility model